“…Dilution of mesityl oxide lowers the extraction. A plot of log D vs. log C mesityl oxide (Figure 1) at 3 and 5M nitric acid indicates slopes of 2.4 and The system conforms to the limiting square law (1) in the case of zirconium (IV). The optimum reagent concentration is 100%.…”
Section: Resultsmentioning
confidence: 58%
“…From 10 runs with 130 µ&., of zirconium (IV), using a general procedure, the average recovery was 96.4 ± 1.2% with a standard deviation of 2.0%. LITERATURE CITED (1) Alcock, K., Bedford, F. C., Hardwick, W. H., McKay, H. A. C., J. Inorg. Nucl.…”
Section: Resultsmentioning
confidence: 99%
“…The modification of this method by Wagner (3), who used titration with barium perchlorate and visual indication with thorin, is considered the best. A recent investigation (1) of the color reaction of sulfonazo III [2, 7-bis-…”
Section: Modification Of Flask Methods Of Sulfur Determinationmentioning
Sir : Mesityl oxide (4-methyl-3penten-2-one) has been used for the extraction of uranium (VI) (2). Extension of these studies to zirconium(IV) revealed that zirconium(IV) can be quantitatively extracted from solutions containing 4M nitric acid and 4M sodium nitrate. Zirconium (IV) is backextracted from the organic phase with water and is spectrophotometrically determined in the aqueous phase with alizarin. This provides the basis for the liquid-liquid extraction of zirconium (IV) at the milligram level. The
“…Dilution of mesityl oxide lowers the extraction. A plot of log D vs. log C mesityl oxide (Figure 1) at 3 and 5M nitric acid indicates slopes of 2.4 and The system conforms to the limiting square law (1) in the case of zirconium (IV). The optimum reagent concentration is 100%.…”
Section: Resultsmentioning
confidence: 58%
“…From 10 runs with 130 µ&., of zirconium (IV), using a general procedure, the average recovery was 96.4 ± 1.2% with a standard deviation of 2.0%. LITERATURE CITED (1) Alcock, K., Bedford, F. C., Hardwick, W. H., McKay, H. A. C., J. Inorg. Nucl.…”
Section: Resultsmentioning
confidence: 99%
“…The modification of this method by Wagner (3), who used titration with barium perchlorate and visual indication with thorin, is considered the best. A recent investigation (1) of the color reaction of sulfonazo III [2, 7-bis-…”
Section: Modification Of Flask Methods Of Sulfur Determinationmentioning
Sir : Mesityl oxide (4-methyl-3penten-2-one) has been used for the extraction of uranium (VI) (2). Extension of these studies to zirconium(IV) revealed that zirconium(IV) can be quantitatively extracted from solutions containing 4M nitric acid and 4M sodium nitrate. Zirconium (IV) is backextracted from the organic phase with water and is spectrophotometrically determined in the aqueous phase with alizarin. This provides the basis for the liquid-liquid extraction of zirconium (IV) at the milligram level. The
“…The system conforms to the limiting square law (1) in the case of zirconium (IV). The optimum reagent concentration is 100%.…”
mentioning
confidence: 72%
“…From 10 runs with 130 µ&., of zirconium (IV), using a general procedure, the average recovery was 96.4 ± 1.2% with a standard deviation of 2.0%. LITERATURE CITED (1) Alcock, K., Bedford, F. C., Hardwick, W. H., McKay, H. A. C., J. Inorg. Nucl.…”
Introduction
Analysis of Azo Compounds
Analysis of Azoxy Compounds
Analysis of Hydrazino Compounds
Azo Compounds as Analytical Tools
Hydrazines as Analytical Tools
Analytical Properties of Analytical Reagents
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