Abstract-Non-metallic objects, such as match box and cigarette box, detection and identification are quite an essential task during personal screening from standoff distance to protect the public places like the airport. Although various imaging sensors such as microwave, THz, infrared and MMW with signal processing techniques have been demonstrated by the researchers for concealed weapon detection, it is still a challenging task to detect and identify different types of small size targets such as matchbox, pocket diary and cigarette box simultaneously. Therefore, in this paper, an attempt has been made to develop such an algorithm/methodology by which different types of small targets, such as a matchbox and cigarette box, which is fully or half-filled or empty and pocket diary at different orientations beneath various cloths can be detected and identified with an MMW radar system. For this purpose, an optimal method has been proposed to form an image, and after that, in post processing a novel adaptive approach for detection and identification of considered targets has been proposed. The data were collected by MMW system at V-band (59 GHz-61 GHz). The proposed algorithm/methodology gives a quite satisfactory result.