Abstract. We test whether X-ray micro-computed tomography (microCT)
imaging can be used as a tool for screening magnetite grains to improve the
accuracy and precision of cosmogenic 3He exposure dating. We extracted
detrital magnetite from a soil developed on a fanglomerate at Whitewater,
California, which was offset by the Banning strand of the San Andreas Fault.
This study shows that microCT screening can distinguish between
inclusion-free magnetite and magnetite with fluid or common solid
inclusions. Such inclusions can produce bulk 3He concentrations that
are significantly in excess of the expected spallation production. We
present Li concentrations, major and trace element analyses, and estimated
magnetite (U–Th) / He cooling ages of samples in order to model the
contribution from fissiogenic, nucleogenic, and cosmogenic thermal neutron
production of 3He. We show that mineral inclusions in magnetite can
produce 3He concentrations of up to 4 times that of the spallation
component, leading to erroneous exposure ages. Therefore, grains with
inclusions must be avoided in order to facilitate accurate and precise
magnetite 3He exposure dating. Around 30 % of all grains were found
to be without inclusions, as detectable by microCT, with the largest
proportion of suitable grains in the grain size range of 400–800 µm.
While grains with inclusions have 3He concentrations far in excess of
the values expected from existing 10Be and 26Al data in quartz at
the Whitewater site, magnetite grains without inclusions have concentrations
close to the predicted depth profile. We measured 3He concentrations in
aliquots without inclusions and corrected them for Li-produced components.
By comparing these data to the known exposure age of 53.5 ± 2.2 ka, we
calibrate a production rate for magnetite 3He at sea level and high latitude (SLHL) of 116 ± 13 at g−1 a−1. We suggest that this microCT screening approach can be
used to improve the quality of cosmogenic 3He measurements of magnetite
and other opaque mineral phases for exposure age and detrital studies.