Control and protection of dispersed photovoltaic power systems integrated into low—voltage distribution feeders

Effects of the concentration of ZrOCI,, calcination temperature, heating rate, and the size of secondary particles after hydrolysis on the preparation of high-purity ZrSiO, fine powders from ZrOCI,.SH,O (0.2M to 1.7M) and equimolar colloidal SiO, using sol-gel processing have been studied. Mechanical properties of the sintered ZrSiO, from the highpurity ZrSiO, powders have been also investigated. Singlephase ZrSiO, fine powders were synthesized at 1300°C by forming ZrSiO, precursors having a Zr-0-Si bond, which was found in all the hydrolysis solutions, and by controlling a secondary particle size after hydrolysis. The conversion rate of ZrSiO, precursor gels to ZrSiO, powders from concentrations other than 0.4M ZrOCI,*SH,O increased when the heating rate was high, whereupon the crystallization of unreacted ZrO, and SiO, was depressed and the propagation and increase of ZrSiO, nuclei in the gels were accelerated. The density of the ZrSiO, sintered bodies, manufactured by firing the ZrSiO, compacts at 1600" to 1700°C, was more than 95% of the theoretical density, and the grain size ranged around 2 to 4 km. The mechanical strength was 320 MPa (room temperature to 1400"C), and the thermal shock resistance was superior to that of mullite and alumina, with fairly high stability at higher temperatures.

show abstract

Preparation of High‐Purity ZrSiO₄ Powder Using Sol–Gel Processing and Mechanical Properties of the Sintered Body

Mori

Yamamura

Kobayashi

et al. 1992

Journal of the American Ceramic Society

View full text Add to dashboard Cite

show abstract

scite is a Brooklyn-based organization that helps researchers better discover and understand research articles through Smart Citations–citations that display the context of the citation and describe whether the article provides supporting or contrasting evidence. scite is used by students and researchers from around the world and is funded in part by the National Science Foundation and the National Institute on Drug Abuse of the National Institutes of Health.

Contact Info

customersupport@researchsolutions.com

10624 S. Eastern Ave., Ste. A-614

Henderson, NV 89052, USA

This site is protected by reCAPTCHA and the Google Privacy Policy and Terms of Service apply.

Blog Terms and Conditions API Terms Privacy Policy Contact Cookie Preferences Do Not Sell or Share My Personal Information

Made with 💙 for researchers

Part of the Research Solutions Family.

Control and protection of dispersed photovoltaic power systems integrated into low—voltage distribution feeders

Cited by 1 publication

References 0 publications

Preparation of High‐Purity ZrSiO₄ Powder Using Sol–Gel Processing and Mechanical Properties of the Sintered Body

Preparation of High‐Purity ZrSiO₄ Powder Using Sol–Gel Processing and Mechanical Properties of the Sintered Body

Contact Info

Product

Resources

About

Control and protection of dispersed photovoltaic power systems integrated into low—voltage distribution feeders

Cited by 1 publication

References 0 publications

Preparation of High‐Purity ZrSiO4 Powder Using Sol–Gel Processing and Mechanical Properties of the Sintered Body

Preparation of High‐Purity ZrSiO4 Powder Using Sol–Gel Processing and Mechanical Properties of the Sintered Body

Contact Info

Product

Resources

About

Preparation of High‐Purity ZrSiO₄ Powder Using Sol–Gel Processing and Mechanical Properties of the Sintered Body

Preparation of High‐Purity ZrSiO₄ Powder Using Sol–Gel Processing and Mechanical Properties of the Sintered Body