2024
DOI: 10.1002/marc.202400416
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Copper‐Free Synthesis of Cationic Glycidyl Triazolyl Polymers

Taichi Ikeda

Abstract: Copper‐free synthesis of cationic glycidyl triazolyl polymers (GTPs) is achieved through a thermal azide‐alkyne cycloaddition reaction between glycidyl azide polymer and propiolic acid, followed by decarboxylation and quaternization of the triazole unit. For synthesizing nonfunctionalized GTP (GTP‐H), a microwave‐assisted method enhances the decarboxylation reaction of carboxy‐functionalized GTP (GTP‐COOH). Three variants of cationic GTPs with different N‐substituents [N‐ethyl, N‐butyl, and N‐tri(ethylene glyc… Show more

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