2023
DOI: 10.1002/ese3.1490
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Correction of sideband effects of nuclear magnetic resonance carbon spectrum in coal and its application in coal structure analysis

Abstract: In the nuclear magnetic resonance (NMR) test of coal, when the spinning frequency of magic‐angle spinning (MAS) is less than the frequency range of chemical shift anisotropy, serious aromatic carbon spinning sidebands will appear. Existing solutions to the sideband effect, such as changing the MAS frequency, inserting total suppression of sidebands (TOSS) pulse sequences, or simply defining the peak after chemical shift of 200 ppm as the sideband peaks generated by aromatic carbon peak, multipling the identifi… Show more

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