Correction of the Distribution Profiles of the Intensities of Elements Considering the Uneven Dispersion of the Glow-Discharge Optical Emission Spectrometer for Multilayer Coatings Analysis

Шулепов, И. А.; Ломыгин, Антон; Laptev, Roman; Kashkarov, Egor; Сыртанов, М. С.

doi:10.1109/efre47760.2020.9241958

Cited by 5 publications

(8 citation statements)

References 13 publications

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“…The layer-by-layer distribution of the Zr, Nb, and H was investigated using glow discharge optical emission spectrometry (GD-OES) on a GD-Profiler 2 spectrometer (Horiba Scientific, France) [34,35]. A two-method approach was used to correct the GD-OES spectra: an initial instrumental selection of the sputtering parameters and a subsequent correction of the spectrum by exponential dependence approximation [36]. NMC Zr/Nb's study was carried out at the following parameters using a radio-frequency source: pressure 650 Pa, power 40 W, frequency 1 kHz, duty cycle 25%.…”

Section: Experimental Methodsmentioning

confidence: 99%

“…The main changes in the relative GD-OES curves are associated with the accumulation Figure 8 shows a GD-OES profile of the Zr/Nb multilayer system consisting of five Zr-layers approximately 80 ± 10 nm thick and five Nb-layers with 100 ± 10 nm thickness, which agrees well with the STEM results (Figure 3). The transient areas between layers present in the GD-OES profiles are related to the crater effect [36,50,51]. The Zr/Nb interface near the Si substrate was not considered.…”

Section: First-principles Calculations Of Zr/nb Multilayer Coatingsmentioning

confidence: 99%

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First-Principles Calculations and Experimental Study of H+-Irradiated Zr/Nb Nanoscale Multilayer System

Laptev

Svyatkin

Krotkevich

et al. 2021

Metals

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Nanoscale multilayer coating (NMC) based on Zr/Nb layers (100/100 nm) before and after H+ irradiation was investigated by combining experimental techniques with first-principles calculations. Detailed studies of structural and phase state and defect structure of Zr/Nb NMC were performed using methods of transmission electron microscopy, X-ray structural analysis, glow discharge optical emission spectrometry, and the Doppler broadening spectroscopy using variable energy positron beam. The first-principles calculations of binding energies for hydrogen in metal Zr/Nb layers was carried out by the pseudopotential method within the density functional theory framework. First-principles calculations and experimental data indicate the presence of macro- and microstrains predominantly in the zirconium layers of Zr/Nb NMC. The main feature of the studied Zr/Nb NMC is the predominant hydrogen localization in Zr layers near the interfaces. The annihilation of positrons is shown to occur mainly in the Zr layers in the vicinity of the interface.

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Section: Experimental Methodsmentioning

confidence: 99%

Section: First-principles Calculations Of Zr/nb Multilayer Coatingsmentioning

confidence: 99%

First-Principles Calculations and Experimental Study of H+-Irradiated Zr/Nb Nanoscale Multilayer System

Laptev

Svyatkin

Krotkevich

et al. 2021

Metals

Self Cite

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“…ИМПУЛЬСНО-ПЛАЗМЕННОЕ МОДИФИЦИРОВАНИЕ ПОВЕРХНОСТИ ДЕТОНАЦИОННЫХ ПОКРЫТИЙ НА ОСНОВЕ Ti-Si-C 1 Рахадилов Б.К., 1 Буйткенов Д.Б., 2 Колиснеченко О.В., 3 Ескермесов Д.К., 3,4 Тоимбаев А.Б. 1 Аманжолов университет, Усть-Каменогорск 2 Институт электросварки имени Е.О.Патона НАН Украины, Киев 3 ТОО «PlasmaScience», Усть-Каменогорск 4 Университет имени Шакарима, Семей…”

Section: Doi: 1017223/978-5-907442-03-0-2021-164unclassified

“…Одним из эффективных технологических путей повышения надежности работы деталей машин и механизмов является нанесение на рабочую поверхность различных покрытий [1]. Однако традиционные методы формирования защитных покрытий (плазменный и детонационный методы напыления порошков и т.…”

Section: Doi: 1017223/978-5-907442-03-0-2021-164unclassified

ИМПУЛЬСНО-ПЛАЗМЕННОЕ МОДИФИЦИРОВАНИЕ ПОВЕРХНОСТИ ДЕТОНАЦИОННЫХ ПОКРЫТИЙ НА ОСНОВЕ Ti–Si–C

2021

Международная Конференция "Физическая Мезомеханика. Материалы С Многоуровневой Иерархически Организованной Структурой И Интелле

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“…The elemental composition of the steel was studied using a Glow Discharge Profiler 2 high-frequency glow discharge optical spectrometer. This laboratory complex combines a glow discharge excited by a radio frequency source and an optical emission spectrometer [28].…”

Section: (D)mentioning

confidence: 99%

Application of the Electrochemical Permeation Method for Hydrogen Diffusion Coefficient Determination in Pipeline Steel 10G2

et al. 2021

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In this article, we conduct research on the effect of corrosion tests on the hydrogen diffusion process in gas steel in electrochemical permeability tests. This tests show that a long corrosion test time reduces the hydrogen diffusion coefficient by an order of magnitude, indicating the formation of aging defects in the steel. During operation, the diffusion coefficient decreases by two orders of magnitude, which also indicates the formation of a large number of defects in the steel. Consequently, based on the change in the diffusion coefficient in the material, it is possible to assess the degree of material failure.

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Correction of the Distribution Profiles of the Intensities of Elements Considering the Uneven Dispersion of the Glow-Discharge Optical Emission Spectrometer for Multilayer Coatings Analysis

Cited by 5 publications

References 13 publications

First-Principles Calculations and Experimental Study of H+-Irradiated Zr/Nb Nanoscale Multilayer System

First-Principles Calculations and Experimental Study of H+-Irradiated Zr/Nb Nanoscale Multilayer System

ИМПУЛЬСНО-ПЛАЗМЕННОЕ МОДИФИЦИРОВАНИЕ ПОВЕРХНОСТИ ДЕТОНАЦИОННЫХ ПОКРЫТИЙ НА ОСНОВЕ Ti–Si–C

Application of the Electrochemical Permeation Method for Hydrogen Diffusion Coefficient Determination in Pipeline Steel 10G2

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