Correction.  Potentiometric Determination of Amides in Acetic Anhydride

Wimer, D. C.

doi:10.1021/ac60135a601

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1964

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“…(8) Kearns, G. L., Maranowski, N. C., Crable, G. F., Ibid., 31, 1646 (1959). (9) Nixon, A. C., Thorpe, R. E., J.…”

Section: Literature Citedmentioning

confidence: 99%

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Spectrophotometric Titration of Primary Aliphatic Amides.

Post¹,

Reynolds²

1964

Anal. Chem.

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gas oils has been reported (1). Their concentration probably never exceeds 1 to 2% weight, and could be corrected for by an independent determination of total oxygen (as in the case of nitrogen compounds). The standard deviation of this method is estimated at ±1 to 2% weight for each class reported, on the basis of multiple determination for several of the samples of Table IV. Linearity in the routine separation was checked for several samples; the recommended sample sizes are less than half the amount necessary to produce appreciable dependence of the analysis results on sample size.

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“…(8) Kearns, G. L., Maranowski, N. C., Crable, G. F., Ibid., 31, 1646 (1959). (9) Nixon, A. C., Thorpe, R. E., J.…”

Section: Literature Citedmentioning

confidence: 99%

“…The lithium aluminum hydride method (8), although relatively specific, requires a steam distillation step after a 15minute reaction period and the pro-cedure cannot be used for dilute aqueous solutions of amides. Nonaqueous acidbase methods (3,9) are not specific for amides, since many other weakly basic substances interfere.…”

Section: Literature Citedmentioning

confidence: 99%

Spectrophotometric Titration of Primary Aliphatic Amides.

Post¹,

Reynolds²

1964

Anal. Chem.

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Correction. Potentiometric Determination of Amides in Acetic Anhydride

Cited by 1 publication

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Spectrophotometric Titration of Primary Aliphatic Amides.

Spectrophotometric Titration of Primary Aliphatic Amides.

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