Creep Behavior of Near α High Temperature Ti-6.6Al-4.6Sn-4.6Zr-0.9Nb-1.0Mo-0.32Si Alloy

Abstract

This study focuses on the microstructure characteristics and tensile and creep properties of a near α high temperature Ti-6.6Al-4.6Sn-4.6Zr-0.9Nb-1.0Mo-0.32Si alloy. Microstructure characteristics were quantitatively investigated using optical microscopy, scanning electron microscope, and transmission electron microscopy. Tensile properties were carried out at room and high temperature. Creep properties were detected under applied stresses ranging from 100–350 MPa at 873–973 K, respectively. Results showed that Widmanstätten microstructure was obtained after hot forged and heat treatment. The strength decreases and the elongation rises with temperature increasing. The ultimate strength and elongation were 1010 MPa, 12% at room temperature, and 620 MPa, 20% at 923 K, respectively. The steady state creep rates rise correspondingly with stress and temperature. Stress exponents are measured within the range of 3.0–3.5. Thus, the creep mechanism is diffusion-controlled viscous glide of dislocation. Ti3Al precipitates are observed. The boundaries and precipitates can obstruct dislocation movement to improve the creep properties. Fracture mechanism of creep is intergranular. The creep mechanism varied from climb of dislocation to sliding of dislocation solution.

Research Progress on the Creep Resistance of High-Temperature Titanium Alloys: A Review

“…Numerous research results show that there are many factors affecting the creep properties of high-temperature titanium alloys [19][20][21], including ambient temperature, applied stress, microstructure, phase size, precipitated phase content and distribution, and impurity element content, as shown in Figure 2. Therefore, this paper mainly focuses on the influence of the above aspects on the creep properties of high-temperature titanium alloys and the possible mechanisms for improving their creep resistance to provide reference for the preparation of high-temperature titanium alloys that can be used at higher temperatures and that have a good match between thermal stability and creep resistance.…”

“…The steady-state creep rate under low stress has a linear relationship with the stress. When Si was added to Ti-6242 alloy to form Ti-6242Si (Ti-6Al-2Sn-4Zr-2Mo-0.07Si) alloy to study the high-temperature creep properties, Es-Souni M, et al [55] [19] conducted high-temperature creep experiments on a new near-α high-temperature titanium alloy: Ti-6.6Al-4.6Sn-4.6Zr-0.9Nb-1.0Mo-0.32Si. The microstructure was quantitatively investigated using optical microscopy (OM), scanning electron microscopy, and TEM.…”