2015
DOI: 10.1063/1.4936413
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Cryogenic distillation facility for isotopic purification of protium and deuterium

Abstract: Isotopic purification of the protium and deuterium is an important requirement of many physics experiments. A cryogenic facility for high-efficiency separation of hydrogen isotopes with a cryogenic distillation column as the main element is described. The instrument is portable, so that it can be used at the experimental site. It was designed and built at the Petersburg Nuclear Physics Institute, Gatchina, Russia. Fundamental operating parameters have been measured including a liquid holdup in the column packi… Show more

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Cited by 22 publications
(5 citation statements)
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“…The TPC allowed in-situ monitoring of impurities by observing charged nuclear recoils from µ − + O → ν µ + N * , in the rare cases of muon transfer to impurities, occuring at the 10 −5 level. Isotopically pure protium was produced onsite [93] and verified by accelerator mass spectroscopy [94]. In total, 1.2 × 10 10 decay events were accepted with muons stopping in the selected restricted fiducial volume.…”
Section: Mucap Experiment: Strategy and Resultsmentioning
confidence: 99%
“…The TPC allowed in-situ monitoring of impurities by observing charged nuclear recoils from µ − + O → ν µ + N * , in the rare cases of muon transfer to impurities, occuring at the 10 −5 level. Isotopically pure protium was produced onsite [93] and verified by accelerator mass spectroscopy [94]. In total, 1.2 × 10 10 decay events were accepted with muons stopping in the selected restricted fiducial volume.…”
Section: Mucap Experiment: Strategy and Resultsmentioning
confidence: 99%
“…The density of the protium gas is ∼1% of liquid hydrogen, thus avoiding the problems involved with meso-molecular processes. A special isotope separation column was constructed for MuCap [9] which removed deuterium to a negligible level. A special gas circulation system [10] was constructed using thermo-dynamical cycles and cryo-absorption by Zeolite filters for continuous cleaning of the protium gas.…”
Section: The Mucap Experimentsmentioning
confidence: 99%
“…The purity is monitored in situ in the TPC by gas chromatography [22]. Isotopically pure deuterium was produced in an on-site cryogenic distillation system [23].…”
Section: Z X Ymentioning
confidence: 99%