Crystal Growth of Deuterated KDP and Determination of the Deuterium Content

Havránková, M.; Březina, B.

doi:10.1002/crat.19740090114

Cryst Res and Technol

1974

DOI: 10.1002/crat.19740090114

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Crystal Growth of Deuterated KDP and Determination of the Deuterium Content

M. Havránková¹,

B. Březina²

Abstract: The relation between the deuterium concentration in the solution and in the solid phase during the growth of K(H, D),PO, crystals a t 30, 45, and 60 "C has been examined.

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1974

1987

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Cited by 7 publications

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The distribution of deuterium between solid and liquid phases during the crystallization of crystals of the KDP group from aqueous solutions

Momtaz

Rashkovich

1976

Phys. Stat. Sol. (a)

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The effect of the deuteration degree of a solution on that of crystallized potassium, rubidium, and cesium dihydrogen phosphates is studied. It is shown that the experimental results can be approxiaated by the equation: XJX, = F + (1 -F ) X,. The quantity "F" characterizes the variation from the equally-probable cam in the distribution of deuterium in a crystal between the groups of D,PO,, HDPO,, and &PO4. This difference decreases with the increase of the ion radius of the cation and the lowering of the solidphase symmetry. The distribution of deuterium in the solution is assumed to be close t o the equally probable one. The effect of crystallization conditions on the distribution coefficient is discussed. I Mayqe~o m m m e cTenem netkrepuposamm pacmopa Ha menem nethepH-POBiiHHH KpEICTaJInH3yIo~KXCR nKrEInpO@OC@lTOB HaJIAx, pY6HAHfl M Ue3Elfl. nOHa3aR0, 9 T O 3KCIIepHMe€iTaJIbHbIe AZWEbIe MOXLIO anp0KCEIMHpOBaTh BbIpaxiemebf X , ] X , = F + (1 -P) X,. BenHsaHa F x a p a~~e p m y e~ oTntIwe B pacnpeneneHuH nePTepm B KpHcTanne Meany rpynnaMa D,PO,, HDPO, EI GPO, KamoHa M nommeHmeM cmme-rpw TsepaoZt aa3b1. IIonaraeTcH, w o pacnpene-~C J I O B M~~ KptrmammaaUtrtI Ha K O~@ $ E I~M~H T pacnpeaenema. OT paB~OBepOHTHOr0. 3 T O OTJIH4He yMeRbIllaeTCH C POCTOM EIOLIHOFO PanHyCa JIeHkie neZbreptrJi B paCTBOpe ~J I H~I E O K paBHOBepORTEOMy. 06cy~cn;ae~cs BJIHH5ie

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The distribution of deuterium between solid and liquid phases during the crystallization of crystals of the KDP group from aqueous solutions

Momtaz

Rashkovich

1976

Phys. Stat. Sol. (a)

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show abstract

Far infrared reflectivity of KDP and KDP-KD*P mixed crystals

et al. 1974

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Growth and characterization of Cs(D1−x, Hx)2 AsO4 from aqueous solutions

Balascio

Loiacono

Hayden

et al. 1975

Materials Research Bulletin

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Crystal Growth of Deuterated KDP and Determination of the Deuterium Content

Abstract: The relation between the deuterium concentration in the solution and in the solid phase during the growth of K(H, D),PO, crystals a t 30, 45, and 60 "C has been examined.

Cited by 7 publications

References 2 publications

The distribution of deuterium between solid and liquid phases during the crystallization of crystals of the KDP group from aqueous solutions

The distribution of deuterium between solid and liquid phases during the crystallization of crystals of the KDP group from aqueous solutions

Far infrared reflectivity of KDP and KDP-KD*P mixed crystals

Growth and characterization of Cs(D1−x, Hx)2 AsO4 from aqueous solutions

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