Crystal structure of 1,3-diaminoimidazolium hexafluorophosphate, [C3H7N4]PF6

Laus, Gerhard; Kahlenberg, Volker; Schottenberger, Herwig

doi:10.1524/ncrs.2010.0203

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“…N,N 1 -Diaminoazolium cations are potent hydrogen bond donors [2,[8][9][10], and it seemed to be of interest to examine the interactions of the 1,4-diamino-1,2,4-triazolium cation with acceptor anions such as sulfate or 5,5′-azotetrazolate in the solid state. The crystal data and refinement details are summarized in Table 1.…”

Section: Resultsmentioning

confidence: 99%

Crystal Structures of Two 1,4-Diamino-1,2,4-triazolium Salts

et al. 2016

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Bis(1,4-diamino-1,2,4-triazolium) sulfate (1) was obtained from the corresponding chloride by ion metathesis using Ag 2 SO 4 . Further metathesis with barium 5,5 1 -azotetrazolate yielded bis(1,4-diamino-1,2,4-triazolium) 5,5 1 -azotetrazolate (2). Numerous NH¨¨¨N and NH¨¨¨O interactions were identified in the crystal structures of 1 and 2. Both compounds undergo exothermal decomposition upon heating.

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Section: Resultsmentioning

confidence: 99%

Crystal Structures of Two 1,4-Diamino-1,2,4-triazolium Salts

et al. 2016

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“…This is the third crystal structure of a1 ,3-diaminoimidazolium salt, the chloride [2]and the hexafluorophosphate [3] have been published previously. It is another example of nitrogen-rich 'energetic salts' which have received much attention [4,5].…”

Section: Discussionmentioning

confidence: 99%