Crystal Structure of 10-Hydroxy-2,6,9-trimethyltricyclo[6,3,01,6]dodeca-9-en-5,11,12-trione (α-Homopipitzolone)

Soriano-Garcı́a, Manuel; Huipe-Nava, Ezequiel; González, Virgilio Mendoza; Garibay, Esther García; Guzmán, J. A.

doi:10.2116/analsci.18.857

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2005

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“…Such a tetracyclic system ( Fig. 1) has not been reported so far, but several compounds contain tricyclic fragments that can be formally derived from the title structure [CSD refcodes PACFOL01 (Fronczek & Caccamese, 1986), WANMAZ (Huipe-Nava et al, 1993), PACFOL (Sims et al, 1971), EGIVAR (Soriano-Garcia et al, 2002) and LAUNIP (Kurata et al, 1981)].…”

Section: Commentmentioning

confidence: 99%

3,5,9,12-Tetra-tert-butyl-10,14-dicyclohexyl-2,8-dioxatetracyclo[5.4.0.2^1,9.1^3,7]tetradeca-4,12-diene-6,11-dione

Meindl¹,

Maslovskaya²,

Noltemeyer³

et al. 2005

Acta Cryst E

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The title compound, C40H62O4, is formed by γ irradiation and contains a tetracyclo[5.4.0.21,9.13,7]tetradecane moiety. The cage consists of bicyclo[2.2.2]octane and bicyclo[3.2.1]octane rings, which are connected via a C—C single bond that is common to both rings. The title compound is formally a dimer of the adduct of a cyclohexyl radical and a 3,5‐di‐tert‐butyl‐ortho‐quinone.

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Section: Commentmentioning

confidence: 99%

3,5,9,12-Tetra-tert-butyl-10,14-dicyclohexyl-2,8-dioxatetracyclo[5.4.0.2^1,9.1^3,7]tetradeca-4,12-diene-6,11-dione

Meindl¹,

Maslovskaya²,

Noltemeyer³

et al. 2005

Acta Cryst E

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show abstract

Crystal Structure of 10-Hydroxy-2,6,9-trimethyltricyclo[6,3,01,6]dodeca-9-en-5,11,12-trione (α-Homopipitzolone)

Cited by 1 publication

References 3 publications

3,5,9,12-Tetra-tert-butyl-10,14-dicyclohexyl-2,8-dioxatetracyclo[5.4.0.2^1,9.1^3,7]tetradeca-4,12-diene-6,11-dione

3,5,9,12-Tetra-tert-butyl-10,14-dicyclohexyl-2,8-dioxatetracyclo[5.4.0.2^1,9.1^3,7]tetradeca-4,12-diene-6,11-dione

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Crystal Structure of 10-Hydroxy-2,6,9-trimethyltricyclo[6,3,01,6]dodeca-9-en-5,11,12-trione (α-Homopipitzolone)

Cited by 1 publication

References 3 publications

3,5,9,12-Tetra-tert-butyl-10,14-dicyclohexyl-2,8-dioxatetracyclo[5.4.0.21,9.13,7]tetradeca-4,12-diene-6,11-dione

3,5,9,12-Tetra-tert-butyl-10,14-dicyclohexyl-2,8-dioxatetracyclo[5.4.0.21,9.13,7]tetradeca-4,12-diene-6,11-dione

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3,5,9,12-Tetra-tert-butyl-10,14-dicyclohexyl-2,8-dioxatetracyclo[5.4.0.2^1,9.1^3,7]tetradeca-4,12-diene-6,11-dione

3,5,9,12-Tetra-tert-butyl-10,14-dicyclohexyl-2,8-dioxatetracyclo[5.4.0.2^1,9.1^3,7]tetradeca-4,12-diene-6,11-dione