2000
DOI: 10.1515/ncrs-2000-0364
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Crystal structure of (1S,2R,5R,6R)-2-methoxy-6-(16-nitrophenylethynyl)-1-azabicyclo[3.2.2]nonane, C17H20N2O3

Abstract: C17H20N2O3, orthorhombic, P2\2\2\ (No. 19), a = 7.096(1) Ä, b= 11.671(1) k,c= 19.277(2) Ä, V= 1596.5 Ä 3 ,Z = 4, R gl (F) = 0.032, wRrefiF 2 ) = 0.040, T= 300 K.Source of material p-N02-Phenyl substituted 10,11-didehydroquincorine [1] was transformed into its corresponding C9-iodide via mesylation and Lil-mediated iodination. The resulting 2-iodomethyl-5-(16-nitrophenylethynyl)-l-azabicyclo[3.2.2]-nonane (500 mg, 1.26 mmol, 1 eq) was dissolved in abs. MeOH (6 ml). After being stirred for 5 min at room temperat… Show more

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