Crystal structure of 3-chloro-N'-(2-hydroxy-3,5-diiodobenzylidene)- benzohydrazide methanol solvate, C14H9ClI2N2O2 · CH3OH

Abstract

C 15 H 13 ClI 2 N 2 O 3 ,triclinic, P1 (no. 2), a =9.057(2) Å,Source of material 2-Hydroxy-3,5-diiodobenzaldehyde (0.1 mmol, 37.4 mg) and 3-chlorobenzohydrazide (0.1 mmol, 17.0 mg) were refluxed in a 30 ml methanol for 30 min to give aclear colorless solution. Colorless block-shaped single crystals of the compound were formed by slow evaporation of the solvent over several days at room temperature. Experimental details