Abstract:Source of material[Cp* 2 Ti(CsC'Bu)] (76 mg, 0.19 mmol) and Co2(CO)8 (65 mg, 0.19 mmol) were dissolved in 5 ml hexane. After 2 days at room temperature the black-orange solution was kept at 195 K. Black crystals appeared which were filtrated and dried in vacuo to afford 123 mg (98%) of the title compound.
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