Crystal structure of bis{μ₂-2,4-dichloro-6-(8-(4-(diethylamino)-2-oxidophenyl)-3,6-dioxa-2,7-diazaocta-1,7-dien-1-yl)phenolato-κ⁵ O:O,N,N′,O′}dicobalt(II) acetone solvate, C₄₃H₄₈Br₄Co₂N₆O₉

Abstract

CCDC no.: 1531179The crystal structure is shown in the figure. Tables 1 and 2 contain details on crystal structure and measurement conditions and a list of the atoms including atomic coordinates and displacement parameters. Source of materialA methanol solution (3.0 mL) of cobalt acetate tetrahydrate (373.5 mg, 0.015 mmol) was added to a acetone solution -(2-(((3,5-dichloro-2-hydroxybenzylidene)amino)oxy)ethyl) oxime (3.96 mg, 0.010 mmol) at room temperature. The color of the solution turned brown immediately. After the mixture was stirred for 1 h, the mixture was filtered. The resulting