Crystal structure of poly-{[μ₂-(E)-1,4-di(1H-imidazol-1-yl)but-2-ene-κ² N:N′][μ₂-cyclohexane-1,4-dicarboxylato-κ⁴ O,O′:O′′,O′′′]nickel(II)}, C₁₈H₂₂N₄NiO₄

Abstract

CCDC no.: 1477897A part of the title crystal structure is shown in the gure. Tables 1 and 2 contain details of the measurement method and a list of the atoms including atomic coordinates and displacement parameters. Source of materialA mixture of cyclohexane-1,4-dicarboxylic acid (0.2 mmol, 0.035 g), (E)-1,4-di(1H-imidazol-1-yl)but-2-ene (0.2 mmol, 0.038 g), NiCl 2 ·6(H 2 O) (0.2 mmol, 0.048 g), and H 2 O (18 mL) was stirred for twenty minutes. The mixtures were transfered in a 30 mL stainless steel reactor with a Te on liner and heated from 293 to 443 K in 4 h and a constant