Crystal structure of methyl 1-(2-(fluorosulfonyl)ethyl)-2-oxocyclopentanecarboxylate, C₉H₁₃FO₅S

Abstract

C 9 H 13 FO5S, triclinic, CCDC no.: 1528194The crystal structure is shown in the figure. Crystal data, data collection and structure refinement details are summarized in Tables 1. Tables 2 lists the Source of materialA mixture of methyl 2-oxocyclopentane carboxylate (20 mg, 1.0 eq), thiourea (N,N-diisopropylethylamine; 0.20 eq) and DIPEA (0.20 eq) was stirred in toluene (1.0 mL) at room