2020
DOI: 10.1515/ncrs-2020-0581
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Crystal structure of tetraaqua-bis(1H-indazole-6-carboxylate-κN)cadmium (II), C16H18CdN4O8

Abstract: C16H18CdN4O8, monoclinic, P21/c (no. 14), a = 6.2751(4) Å, b = 21.7902(13) Å, c = 13.3401(8) Å, β = 90.793(1)°, V = 1823.89(19) Å3, Z = 4, Rgt(F) = 0.0252, wRref(F2) = 0.0603, T = 296(2) K.

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“…Subsequent work has shown versatile coordination behaviour in other indazole-carboxylic acid isomers, although still more commonly coordinating in their monoanionic (N-H) forms. 43 Introducing additional heterocyclic functionality on the fused six-membered ring gives access to a family of ligands not only with lower pK a , and thus with more tendency towards in-situ deprotonation, but also with more compact and geometrically controlled coordination geometries. We recently reported the coordination chemistry of the isomeric pair of ligands pyrazolo[4,3-b]pyridine (4-azaindazole) and pyrazolo[3,4c]pyridine (6-azaindazole), HL6 and HL7 respectively.…”
Section: Indazolesmentioning
confidence: 99%
“…Subsequent work has shown versatile coordination behaviour in other indazole-carboxylic acid isomers, although still more commonly coordinating in their monoanionic (N-H) forms. 43 Introducing additional heterocyclic functionality on the fused six-membered ring gives access to a family of ligands not only with lower pK a , and thus with more tendency towards in-situ deprotonation, but also with more compact and geometrically controlled coordination geometries. We recently reported the coordination chemistry of the isomeric pair of ligands pyrazolo[4,3-b]pyridine (4-azaindazole) and pyrazolo[3,4c]pyridine (6-azaindazole), HL6 and HL7 respectively.…”
Section: Indazolesmentioning
confidence: 99%