Abstract:Source of materialThec ompound was obtained upon reaction of bis(3-formyl-4-hydroxyphenyl)methane and trans-ReOBr 3 (PPh 3 ) 2 in ethanol. Crystals suitablefor thediffraction studywereobtaineduponfree evaporationofthe solventatambient conditions.
Experimental detailsCarbon-boundHatoms were placed in calculated positions(C-H =0.95Åfor aromatic carbon atoms, C-H=0.99Åfor themethylene group) andw erei ncludedi nt he refinement in the riding model approximation, with U iso (H) setto1.2U eq (C). The Hatoms of the m… Show more
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