2015
DOI: 10.1515/ncrs-2014-0252
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Crystal structure of trans-dibromido-ethoxido-oxido-bis(triphenylphosphane)- rhenium(V) – a triclinic polymorph, C38H35Br2O2P2Re

Abstract: Source of materialThec ompound was obtained upon reaction of bis(3-formyl-4-hydroxyphenyl)methane and trans-ReOBr 3 (PPh 3 ) 2 in ethanol. Crystals suitablefor thediffraction studywereobtaineduponfree evaporationofthe solventatambient conditions. Experimental detailsCarbon-boundHatoms were placed in calculated positions(C-H =0.95Åfor aromatic carbon atoms, C-H=0.99Åfor themethylene group) andw erei ncludedi nt he refinement in the riding model approximation, with U iso (H) setto1.2U eq (C). The Hatoms of the m… Show more

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