2016
DOI: 10.1063/1.4941442
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Cubic to tetragonal phase transition of Tm3+ doped nanocrystals in oxyfluoride glass ceramics

Abstract: Tm3+ ions doped β-PbF2 nanocrystals in oxyfluoride glass ceramics with different doping concentrations and thermal temperatures are prepared by a traditional melt-quenching and thermal treatment method to investigate the structure and the phase transition of Tm3+ doped nanocrystals. The structures are characterized by X-ray diffraction Rietveld analysis and confirmed with numerical simulation. The phase transitions are proved further by the emission spectra. Both of the doping concentration and thermal tempera… Show more

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Cited by 6 publications
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“…14,35 But for ternary/quaternary compounds, the phase change is observed with the increase of one of the constituents. [36][37][38] For Rietveld analysis, the oxygen positions were considered as free parameters.…”
Section: Resultsmentioning
confidence: 99%
“…14,35 But for ternary/quaternary compounds, the phase change is observed with the increase of one of the constituents. [36][37][38] For Rietveld analysis, the oxygen positions were considered as free parameters.…”
Section: Resultsmentioning
confidence: 99%