2015
DOI: 10.1063/1.4935586
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Dancing the tight rope on the nanoscale—Calibrating a heat flux sensor of a scanning thermal microscope

Abstract: We report on a precise in situ procedure to calibrate the heat flux sensor of a near-field scanning thermal microscope. This sensitive thermal measurement is based on 1ω modulation technique and utilizes a hot wire method to build an accessible and controllable heat reservoir. This reservoir is coupled thermally by near-field interactions to our probe. Thus, the sensor's conversion relation V(th)(Q(GS)*) can be precisely determined. V(th) is the thermopower generated in the sensor's coaxial thermocouple and Q(… Show more

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Cited by 2 publications
(3 citation statements)
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“…The details of this calibration method can be found in ref. 35 . For the NSThM probe used in our measurements we find a calibration factor of ε =0.43 μW per μV.…”
Section: Methodsmentioning
confidence: 99%
See 1 more Smart Citation
“…The details of this calibration method can be found in ref. 35 . For the NSThM probe used in our measurements we find a calibration factor of ε =0.43 μW per μV.…”
Section: Methodsmentioning
confidence: 99%
“…Our calibration method enables us to measure absolute heat fluxes between the probe and the sample with a relative uncertainty of about 14% (details of the error analysis leading to this uncertainty can be found in ref. 35 ).…”
Section: Methodsmentioning
confidence: 99%
“…Experimental data on heat transfer between a tip and a planar sample. The data were taken with thermal scanning microscopes [10,22] that allow for a simultaneous measurement of the electronic tunnelling current (onset at distances shorter than d ∼ 0.5−1 nm, right scale). The shaded areas illustrate the typical measurement uncertainties.…”
Section: Model For Experimental Datamentioning
confidence: 99%