2023
DOI: 10.26434/chemrxiv-2023-stbm1-v2
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Deciphering the Interplay Between Local and Global Dynamics of Anodic Metal Oxidation

Aleksei Makogon,
Jean-Marc Noël,
Frédéric Kanoufi
et al.

Abstract: The stark difference between global and local metal oxidation dynamics underscores the need for methodologies capable of performing precise sub-µm-scale and wide-field measurements. In this study, we present Reflective Microscopy (RM) as a tool developed to address this challenge, illustrated by the example of chronoamperometric Fe oxidation in NaCl solution. Analysis at a local scale of 10s of µm has revealed three distinct periods of Fe oxidation: the initial covering of the metal interface with a surface fi… Show more

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