Decomposition method in semi-closed system with cold finger for evaluation of Ca, K, Na, Mg, Zn and Fe in colostrum silage by F AAS and F AES

Pereira, Clairton Marcolongo; Vitola, Helena Reissig Soares; Souza, Alexander Ossanes de; Medina, Aline Lisbôa; Gularte, Márcia Arocha; Ribeiro, Anderson Schwingel

doi:10.1016/j.microc.2016.07.012

Cited by 5 publications

(2 citation statements)

References 19 publications

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“… n.f. 5.7 a 148 , 1.1 a 148 0.8 119 –3.6 119 K 2.9 0.7–9.4 a 149 4–7 a 145 0.6 35 –4.7 13 1.2 119 –3.1 119 Ca 5.4 0.7–4.3 a 150 n.f. 2.0 35 –6 16 1.2 90 –9.5 119 Fe 5.1 1.2–10.0 a 149 < 7 a 151 0.5 83 –25 25 1.13 96 –4.1 90 Cu 5.7 3.4 a 152 , 7.2 a 152 1.29 60 –7.35 60 0.6 83 –11.1 26 0.7 100 –9.7 89 Zn 4.1 0.8–8.6 a 149 8–15 a 153 ...…”

Section: Evaluation Of the Usefulness Of The Total Reflection X-ray Fmentioning

confidence: 99%

The assessment of the usability of selected instrumental techniques for the elemental analysis of biomedical samples

Planeta

Kubala‐Kukuś

Dróżdż

et al. 2021

Sci Rep

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The fundamental role of major, minor and trace elements in different physiological and pathological processes occurring in living organism makes that elemental analysis of biomedical samples becomes more and more popular issue. The most often used tools for analysis of the elemental composition of biological samples include Flame and Graphite Furnace Atomic Absorption Spectroscopy (F-AAS and GF-AAS), Inductively Coupled Plasma Optical Emission Spectroscopy (ICP-OES) and Inductively Coupled Plasma Mass Spectrometry (ICP-MS). Each of these techniques has many advantages and limitations that should be considered in the first stage of planning the measurement procedure. Their reliability can be checked in the validation process and the precision, trueness and detection limits of elements belong to the most frequently determined validation parameters. The main purpose of this paper was the discussion of selected instrumental techniques (F-AAS, GF-AAS, ICP-OES and ICP-MS) in term of the achieved validation parameters and the usefulness in the analysis of biological samples. The focus in the detailed literature studies was also put on the methods of preparation of the biomedical samples. What is more based on the own data the usefulness of the total reflection X-ray fluorescence spectroscopy for the elemental analysis of animal tissues was examined. The detection limits of elements, precision and trueness for the technique were determined and compared with the literature data concerning other of the discussed techniques of elemental analysis. Reassuming, the following paper is to serve as a guide and comprehensive source of information concerning the validation parameters achievable in different instrumental techniques used for the elemental analysis of biomedical samples.

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Section: Evaluation Of the Usefulness Of The Total Reflection X-ray Fmentioning

confidence: 99%

The assessment of the usability of selected instrumental techniques for the elemental analysis of biomedical samples

Planeta

Kubala‐Kukuś

Dróżdż

et al. 2021

Sci Rep

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“…The Na and K content of lean beef and beef kidney were determined using a flame-atomic absorption spectrophotometer produces a large quantity of free electrons in the flame due to cesium's low ionization energy, which in turn suppresses the ionization of sodium and potassium and thus their mutual interferences can be neglected 35 . For quantification, calibration curves were obtained using standard solutions of sodium (cat.…”

Section: Atomic Absorption Spectroscopy Analysismentioning

confidence: 99%

Laser induced breakdown spectroscopy for quantification of sodium and potassium in minced beef: a potential technique for detecting beef kidney adulteration

et al. 2017

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Recommended Citation Dixit, Y. et al (2017). Laser induced breakdown spectroscopy for quantification of sodium and potassium in minced beef: a potential technique for detecting beef kidney adulteration. Analytical Methods, vol. 9, pg. 3314-3322. doi:10.1039/C7AY00757D Authors Y. Dixit, Maria Piedad Casado-Gavalda, R. Cama-Moncunill, X. Cama-Moncunill, Maria Markiewicz-Kȩszycka, Patrick Cullen, and Carl Sullivan Beef is a rich source of important minerals, with potassium (K) being the most abundant mineral quantitatively except in cured meats where Na from the added salt predominates. This study evaluates the potential of LIBS for quantification of the sodium (Na) and potassium (K) contents of minced beef as a potential method of detecting beef kidney adulteration. Additionally, the study aims at demonstrate the ability of LIBS to provide spatial mineral information of minced beef. A LIBS system was employed to collect spectral information of adulterated minced beef samples. Atomic absorption spectroscopy (AAS) was used to obtain reference values for Na and K. The chemometric technique of partial least squares regression (PLSR) was used to build the prediction models. Spatial mineral maps of minced beef samples were generated based on the predicted percentages of Na and K. The models for Na and K yielded calibration coefficients of determination ( 2 )

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Corrosion Behavior of Bitter Almond Oil During Processing

Mao

Zhu

Zhao

et al. 2019

Euro J Lipid Sci & Tech

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This study aims to explore the corrosion behavior of bitter almond oil (BAO) during processing. Hydrocyanic acid (HCN) and benzoic acid in oil are speculated as the main components that corrode the screw oil expeller. Immersion and simulation corrosion tests are carried out to verify this hypothesis. Immersion test results show that crude BAO (CBAO) containing 5.07 ± 0.06 mg kg−1 benzoic acid and 4.25 ± 0.04 mg kg−1 HCN exhibits corrosive effects on steel. Simulation corrosion test results indicate that the addition of CN− or benzoic acid has significant effect on the corrosion of steel. Specifically, at ≥1 × 104 mg kg−1 benzoic acid concentration or ≥5 mg kg−1 CN− concentration, the mass of steel blocks in oil decreases and the contents of Fe, Zn, Al, and Mg ions in oil increase significantly. Therefore, HCN in CBAO is the main cause of screw oil expeller corrosion in BAO processing and benzoic acid is the secondary cause. Practical Applications: The corrosion behavior of CBAO not only damages the integrity of the screw oil expeller but also increases the dissolution of toxic metals from the components into oil. The study of corrosion has practical value in taking effective measures, such as detoxification before pressing and addition of natural inhibitors, to reduce corrosion and ensure the quality of CBAO. Corrosion study provides the basis for the selection of steel materials of screw oil expeller.

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Decomposition method in semi-closed system with cold finger for evaluation of Ca, K, Na, Mg, Zn and Fe in colostrum silage by F AAS and F AES

Cited by 5 publications

References 19 publications

The assessment of the usability of selected instrumental techniques for the elemental analysis of biomedical samples

The assessment of the usability of selected instrumental techniques for the elemental analysis of biomedical samples

Laser induced breakdown spectroscopy for quantification of sodium and potassium in minced beef: a potential technique for detecting beef kidney adulteration

Corrosion Behavior of Bitter Almond Oil During Processing

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