Defocusing correction for the measurement of preferred orientation

Wilson, D.J.; Bainbridge, D. W.

doi:10.1007/bf02813272

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1974

2015

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Cited by 5 publications

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“…One should, therefore, be cautious before applying it. Instead of random specimens for establishing the defocusing effects, Wilson & Bainbridge (1971) used specimens with known textural symmetry. The texture at equal positions from e.g.…”

Section: Ibkrmentioning

confidence: 99%

Defocusing effects in the reflexion technique for the determination of preferred orientation

Huijser-Gerits¹,

Rieck²

1974

J Appl Cryst

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The defocusing of the diffracted beam in a texture goniometer using the reflexion technique for the determination of the preferred orientation is discussed. By means of textureless (random) specimens of the ferromagnetic material Ba3CozFez.,O4~ this defocusing is measured for several diffraction planes in two cases: (1) a narrow and (2) a wide receiving slit. Calibration functions to correct for defocusing effects are calculated using an equation given by Gale & Griffiths [ Brit. J. Appl. Phys. (1960). 11, 96-102]. The calculated functions plotted rersus the angle of specimen tilt are compared with the relative intensities measured on random specimens.

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Section: Ibkrmentioning

confidence: 99%