Design of powder diffraction beamline (BL-I11) at Diamond

Tang, C. C. H.; Thompson, Stephen P.; Hill, T. P.; Wilkin, Guy; Wagner, U.

doi:10.1524/zksu.2007.2007.suppl_26.153

Cited by 28 publications

(56 citation statements)

References 3 publications

Supporting

Mentioning

Contrasting

Order By: Relevance

“…Where possible, single crystal X-ray diffraction was performed. Additional structural information was derived from synchrotron X-ray powder diffraction, when single crystals could not be obtained, either at station ID-31, ESRF [24], or at station I-11, Diamond Light Source, Rutherford Appleton laboratory [25] (details in the ESI).…”

Section: Methodsmentioning

confidence: 99%

Lanthanide N,N′-piperazine-bis(methylenephosphonates) (Ln=La, Ce, Nd) that display flexible frameworks, reversible hydration and cation exchange

Mowat

Groves

Wharmby

et al. 2009

Journal of Solid State Chemistry

View full text Add to dashboard Cite

Section: Methodsmentioning

confidence: 99%

Lanthanide N,N′-piperazine-bis(methylenephosphonates) (Ln=La, Ce, Nd) that display flexible frameworks, reversible hydration and cation exchange

Mowat

Groves

Wharmby

et al. 2009

Journal of Solid State Chemistry

View full text Add to dashboard Cite

“…The synchrotron X-ray diffraction work was carried out with the support of the Diamond Light Source. Specifically, KMK and AS would like to thank Dr Julia E. Parker and her colleagues in the team on Beamline I11 at Diamond (Tang et al, 2007;Thompson et al, 2009) for undertaking the X-ray synchrotron radiation experiments on the sample of M phase powder that we provided for proposal Rapid Access EE4111. BS and MW would like to thank Katharina Scheidl for assistance during the single-crystal growth experiments.…”

Section: Acknowledgementsmentioning

confidence: 99%

Crystal structure of the thortveitite-relatedMphase, (Mn_xZn_1–x)₂V₂O₇(0.75 <x< 0.913): a combined synchrotron powder and single-crystal X-ray study

et al. 2018

View full text Add to dashboard Cite

Supporting information: this article has supporting information at journals.iucr.org/c Crystal structure of the thortveitite-related M phase, (Mn x Zn 1-x ) 2 V 2 O 7 (0.75 < x < 0.913): a combined synchrotron powder and single-crystal X-ray studyThe determination of the crystal structure of the M phase, (Mn x Zn 1-x ) 2 V 2 O 7 (0.75 < x < 0.913), in the pseudobinary Mn 2 V 2 O 7 -Zn 2 V 2 O 7 system for x ' 0.8 shows that the previously published triclinic unit-cell parameters for this thortveitite-related phase do not describe a true lattice for this phase. Instead, single-crystal X-ray data and Rietveld refinement of synchrotron X-ray powder data show that the M phase has a different triclinic structure in the space group P1 with Z = 2. As prior work has suggested, the crystal structure can be described as a distorted version of the thortveitite crystal structure of -Mn 2 V 2 O 7 . A twofold superstructure in diffraction patterns of crystals of the M phase used for single-crystal X-ray diffraction work arises from twinning by reticular pseudomerohedry. This superstructure can be described as a commensurate modulation of a pseudo-monoclinic basis structure closely related to the crystal structure of -Mn 2 V 2 O 7 . In comparison with the distortions introduced when -Mn 2 V 2 O 7 transforms at low temperature to -Mn 2 V 2 O 7 , the distortions which give rise to the M phase from the -Mn 2 V 2 O 7 prototype are noticeably less pronounced. research papers 1080 Knowles et al. Crystal structure of a thortveitite-related M phase Knowles et al. Crystal structure of a thortveitite-related M phase 1087 supporting information sup-1

show abstract

“…The technical design was peer reviewed in July 2005 and the beamline is now entering user operations. The key features and specifications of the beamline design, prior to construction, are summarized in Tang et al 9 We present here the results of performance benchmarking for the high resolution a͒ measurement mode of the new I11 powder instrument, along with details of the x-ray beam and beamline performance characteristics.…”

Section: Introductionmentioning

confidence: 99%

Beamline I11 at Diamond: A new instrument for high resolution powder diffraction

Thompson

Parker

Potter

et al. 2009

Review of Scientific Instruments

Self Cite

325

230

View full text Add to dashboard Cite

The performance characteristics of a new synchrotron x-ray powder diffraction beamline (I11) at the Diamond Light Source are presented. Using an in-vacuum undulator for photon production and deploying simple x-ray optics centered around a double-crystal monochromator and a pair of harmonic rejection mirrors, a high brightness and low bandpass x-ray beam is delivered at the sample. To provide fast data collection, 45 Si(111) analyzing crystals and detectors are installed onto a large and high precision diffractometer. High resolution powder diffraction data from standard reference materials of Si, alpha-quartz, and LaB6 are used to characterize instrumental performance.

show abstract

Design of powder diffraction beamline (BL-I11) at Diamond

Cited by 28 publications

References 3 publications

Lanthanide N,N′-piperazine-bis(methylenephosphonates) (Ln=La, Ce, Nd) that display flexible frameworks, reversible hydration and cation exchange

Lanthanide N,N′-piperazine-bis(methylenephosphonates) (Ln=La, Ce, Nd) that display flexible frameworks, reversible hydration and cation exchange

Crystal structure of the thortveitite-relatedMphase, (Mn_xZn_1–x)₂V₂O₇(0.75 <x< 0.913): a combined synchrotron powder and single-crystal X-ray study

Beamline I11 at Diamond: A new instrument for high resolution powder diffraction

Contact Info

Product

Resources

About

Design of powder diffraction beamline (BL-I11) at Diamond

Cited by 28 publications

References 3 publications

Lanthanide N,N′-piperazine-bis(methylenephosphonates) (Ln=La, Ce, Nd) that display flexible frameworks, reversible hydration and cation exchange

Lanthanide N,N′-piperazine-bis(methylenephosphonates) (Ln=La, Ce, Nd) that display flexible frameworks, reversible hydration and cation exchange

Crystal structure of the thortveitite-relatedMphase, (MnxZn1–x)2V2O7(0.75 <x< 0.913): a combined synchrotron powder and single-crystal X-ray study

Beamline I11 at Diamond: A new instrument for high resolution powder diffraction

Contact Info

Product

Resources

About

Crystal structure of the thortveitite-relatedMphase, (Mn_xZn_1–x)₂V₂O₇(0.75 <x< 0.913): a combined synchrotron powder and single-crystal X-ray study