2019
DOI: 10.3724/sp.j.1123.2018.10038
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Determination of acrylamide in coffee by ultra performance liquid chromatography-atmospheric pressure chemical ionization tandem mass spectrometry

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Cited by 3 publications
(4 citation statements)
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“… 6.3 97.4–108.4 0-300 R2: 0.997 LOD: 10 LOQ: 20.5 [ 36 ] UHPLC-MS/MS Column: C18 SPE N.I. 2.8–3.6 94.6–115 100-1000 R2: 0.99 LOD: 5 LOQ: 10 [ 57 ] Coffee and cocoa HPLC-MS/MS Column: PGC SPE 0.6–2.5 9.00 102.9 98-25000 R2: 0.99998 N.I. [ 26 ] HPLC-MS/MS Column: PMA SPE 5.4–15.8 7.7–22.8 N.I.…”
Section: Extraction Techniques Of Neo-formed Compounds Present In Cof...mentioning
confidence: 99%
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“… 6.3 97.4–108.4 0-300 R2: 0.997 LOD: 10 LOQ: 20.5 [ 36 ] UHPLC-MS/MS Column: C18 SPE N.I. 2.8–3.6 94.6–115 100-1000 R2: 0.99 LOD: 5 LOQ: 10 [ 57 ] Coffee and cocoa HPLC-MS/MS Column: PGC SPE 0.6–2.5 9.00 102.9 98-25000 R2: 0.99998 N.I. [ 26 ] HPLC-MS/MS Column: PMA SPE 5.4–15.8 7.7–22.8 N.I.…”
Section: Extraction Techniques Of Neo-formed Compounds Present In Cof...mentioning
confidence: 99%
“…This can be counteracted by employing deuterated isotopes and discussed sample preparation (Section 2 ), quantifying AA and AA-d3 with a mass-to-charge ratio of m / z = 72 > 55 and m / z = 75 > 58 [ 26 ]. Electrospray ionisation and atmospheric pressure chemical ionisation are widely used ionisation sources, suitable for a broad molecular weight range and high polarity analytes [ 26 , 56 , 57 ]. Moreover, organic modifiers such as acetic acid, formic acid, and galli c acid are common in the mobile phase for AA determination.…”
Section: Analytical Techniques For Nfcs Quantification In Cacao and R...mentioning
confidence: 99%
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“…Moreover, the expensive technology and equipment limit its applications. The use of high performance liquid chromatography has simplified this analysis [9,10]. This method is carried out at room temperature and overcomes the thermal instability of acrylamide.…”
Section: Introductionmentioning
confidence: 99%