2014
DOI: 10.1016/j.coal.2014.01.002
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Determination of As and Se in coal and coal combustion products using closed vessel microwave digestion and collision/reaction cell technology (CCT) of inductively coupled plasma mass spectrometry (ICP-MS)

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Cited by 137 publications
(65 citation statements)
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“…Details for these coal-related sample digestion and ICP-MS analysis techniques are given by Dai et al [1]. Arsenic and selenium were determined by ICP-MS, using collision cell technology (CCT), in order to avoid disturbance of polyatomic ions [24].…”
Section: Samples and Analytical Proceduresmentioning
confidence: 99%
“…Details for these coal-related sample digestion and ICP-MS analysis techniques are given by Dai et al [1]. Arsenic and selenium were determined by ICP-MS, using collision cell technology (CCT), in order to avoid disturbance of polyatomic ions [24].…”
Section: Samples and Analytical Proceduresmentioning
confidence: 99%
“…ICP-MS parameters have an accuracy and precision which deviate by less than 5% from the reference standard values. More details of ICP-MS analysis and its method detection limits for various trace elements were described by Dai et al [23,24] and Li et al [25]. Mercury was determined using a Milestone DMA-80 analyzer.…”
Section: Introductionmentioning
confidence: 99%
“…Inductively coupled plasma mass spectrometry (ICP-MS, Thermofisher X series II, Thermo Fisher Scientific), in pulse counting mode (three points per peak), was used to determine trace element concentrations in the samples, except for Hg and F. The ICP-MS analysis and sample microwave digestion program are outlined by Dai et al [24]. Arsenic and Se were determined by ICP-MS using collision cell technology (CCT) in order to avoid disturbance of polyatomic ions [25]. For ICP-MS analysis, samples were digested using an UltraClave Microwave High Pressure Reactor (Milestone Inc., Shelton, CT, USA).…”
Section: Introductionmentioning
confidence: 99%
“…Multi-element standards (Inorganic Ventures: CCS-1, CCS-4, CCS-5 and CCS-6) were used for the calibration of trace element concentrations [24]. Arsenic and Se were analyzed via ICP-MS with collision/reaction cell technology (ICP-CCT-MS) [25]. Fluorine was determined via pyrohydrolysis combined with an ionselective electrode (ISE) based on the ASTM method [26].…”
Section: Samples and Methodsmentioning
confidence: 99%