Determination of chloramphenicol, enrofloxacin and 29pesticides residues in bovine milk by liquid chromatography–tandem mass spectrometry

Tian, Hongzhe

doi:10.1016/j.chemosphere.2010.12.016

Cited by 60 publications

(35 citation statements)

References 23 publications

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“…Organochlorine pesticides were extensively used to increase the production of agricultural crops by preventing losses due to pest [15]. Worldwide production and use of Organochlorine compounds (OCs) since 1950s have resulted in their widespread occurrence in the environment.…”

Section: Introductionmentioning

confidence: 99%

Quantification of Organochlorine Pesticide Residues in the Buffalo Milk Samples of Delhi City, India

Aslam¹,

Rais²,

Alam³

2013

JEP

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The ill effects of green revolution include residues of extensively used chemical pesticides in various environmental components. The present study was designed to analyze the levels of organochlorine pesticide residues along with chemical composition in buffalo milk samples collected from different localities of Delhi. Milk monitoring can yield information about the kinds and quantities of pesticides in the environment as well as in our daily diet. In this study, the residue of three different organochlorine pesticides, namely Hexachlorocyclohexane (HCH), Dichlorodiphenyltrichloroethane (DDT) and Endosulfan have been reported. Residues of Lindane exceeded the Maximum Residual Limit values in 50% of the samples is a cause of serious concern. The p,p'-DDT was detected in 70% of the samples with p,p'-DDE (dichlorodiphenyldichloroethylene) in 80% of the milk samples of different parts of Delhi state. DDD (Dichlorodiphenyldichloroethane) another metabolite of p,p'-DDT was detected in 65% of the milk samples. The analysis indicates that DDT is the major contaminants in different parts of Delhi state. α and β endosulfan were detected in 35% and 40% of the samples analyzed. The statistical correlation shows no significant correlation between chemical compositions of the samples. The presence of multiple chemicals in virtually all samples of buffalo milk raises new questions about the possible toxicological impacts of chemical mixtures on an infant's developing nervous and immune systems and reproductive organs.

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Section: Introductionmentioning

confidence: 99%

Quantification of Organochlorine Pesticide Residues in the Buffalo Milk Samples of Delhi City, India

Aslam¹,

Rais²,

Alam³

2013

JEP

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“…Its sample purity requirements are not stringent, and it enables a simultaneous analysis of substances that vary considerably in polarity. The popularity of the method is confirmed by the increasing number of publications dedicated to the applications of LC-MS in the determination of contaminants, including pesticides, in food (Sivaperumal et al 2015;Gómez-Pérez et al 2015;Martinez-Dominguez et al 2015;Golge and Kebak 2015;Fillatre et al 2014;Esturk et al 2014;Oshita and Jardim 2014;González-Curbelo et al 2014;Rajski et al 2013;Arienzo et al 2013;Stachniuk and Fornal 2013;Sinha et al 2012;Gilbert-Lopez et al 2012;Lozano et al 2012;Chung and Lam 2012;BoteroCoy et al 2012;Tian 2011;Pareja et al 2011;Kmellar et al 2011;Aguilera-Luiz et al 2011;Chen et al 2011;Lehotay et al 2010;Zhang et al 2010;Camino-Sanchez et al 2010;Kamel et al 2010;Brutti et al 2010). In pesticide residue analysis, similarly to the analysis of other food contaminants, there is a distinct tendency to develop fast multiresidue methods.…”

Section: Introductionmentioning

confidence: 87%

“…Alongside the quadrupole analyzer, the ion trap analyzer is one of the most popular single MS analyzers in the analysis of pesticide residues in food (Tian 2011;Brutti et al 2010;Radisic et al 2009;Lesueur et al 2008;Wang et al 2007;Soler et al 2007). …”

Section: Ion Trap Analyzermentioning

confidence: 99%

Liquid Chromatography-Mass Spectrometry in the Analysis of Pesticide Residues in Food

2015

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The analysis of pesticide residues in food is nowadays an increasingly important task. Quality control has to be very strict in order to safeguard the consumers' health. One of the most important goals of food quality assurance is testing food for residues and contaminants. Among chemical hazards, the contamination of food with pesticides has been characterized as a significant source of many serious diseases. Consumption of food containing pesticide residues may cause cancer, malformations, and damage to the endocrine, nervous, and immune system. In order to assure human food safety, The European Community has established maximum residue limits (MRL) of pesticides permitted in products of animal or vegetable origin that are intended for human consumption. In the EU, Regulation (EC) No. 396/2005 of the European Parliament and Council on pesticide residues established the levels of pesticide residues allowed in food and feed. To ensure the compliance of marketed food commodities with the law on food safety, sensitive and reliable analytical methods for the determination of pesticide residues are required. Multiresidue liquid chromatography-mass spectrometry methods (LC-MS) are widely recognized as an ideal, highly specific, and extremely sensitive technique for testing food products. This review discusses LC-MS approaches applied most widely to pesticide residue analysis over the last few years. The main ionization methods and MS detectors used as analytical tools in quantification and/or identification/confirmation of pesticide residues in food are presented.

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“…[11][12][13] Determination of pesticides in different sample matrices is usually performed after pretreatment steps using either gas chromatography (GC)-mass spectrometry (MS), 14 GC-electron capture and ion trap mass spectrometric detectors, 15 GCnitrogen-phosphorus detector, 16 GC-flame photometric detector, 17 GC-flame ionization detector, 18 or high performance liquid chromatography (HPLC) with different detectors (e.g. MS/MS spectrometry, 19 diode array detector). 20 The use of ultraperformance liquid chromatography in detection of pesticides has also been reported.…”

Section: Introductionmentioning

confidence: 99%

Simultaneous determination of permethrin and deltamethrin in water samples by magnetic solid-phase extraction coupled with dispersive liquid-liquid microextraction combined with gas chromatography

et al. 2017

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In this study, new and efficient method, magnetic solid phase extraction coupled with dispersive liquid-liquid microextracton (MSPE-DLLME) combined with gas chromatography-flame ionization detector (GC-FID) was developed for the preconcentration and determination of permethrin and deltamethrin in water samples. KEYWORDSMagnetic solid-phase extraction, dispersive liquid-liquid microextraction, permethrin, deltamethrin, gas chromatography, water samples IntroductionInsecticides on the basis of pyrethrine were first introduced in the 1950s. Pyrethrines are a class of natural substances which originates from the blossom of the chrysanthemum. Pyrethrines were, and still are, used as natural insecticides against vermin in households. Nevertheless, the production of pyrethrine is expensive and the resources are limited. For these reasons synthetic pyrethroids were developed based on the basic structure of natural pyrethrines.

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Determination of chloramphenicol, enrofloxacin and 29pesticides residues in bovine milk by liquid chromatography–tandem mass spectrometry

Cited by 60 publications

References 23 publications

Quantification of Organochlorine Pesticide Residues in the Buffalo Milk Samples of Delhi City, India

Quantification of Organochlorine Pesticide Residues in the Buffalo Milk Samples of Delhi City, India

Liquid Chromatography-Mass Spectrometry in the Analysis of Pesticide Residues in Food

Simultaneous determination of permethrin and deltamethrin in water samples by magnetic solid-phase extraction coupled with dispersive liquid-liquid microextraction combined with gas chromatography

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