1992
DOI: 10.1016/0378-4347(92)80309-e
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Determination of chloramphenicol in muscle using a particle beam interface for combining liquid chromatography with negative-ion chemical ionization mass spectrometry

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Cited by 18 publications
(5 citation statements)
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“…According to the criteria, the recoveries at those levels should range from 70 to 110%. Our results show the accuracy and repeatability of the MSPD method to be fully comparable to those of the highly efficient methods described by Hummert et al (7) and Delepine et al (9).…”
Section: Discussionsupporting
confidence: 85%
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“…According to the criteria, the recoveries at those levels should range from 70 to 110%. Our results show the accuracy and repeatability of the MSPD method to be fully comparable to those of the highly efficient methods described by Hummert et al (7) and Delepine et al (9).…”
Section: Discussionsupporting
confidence: 85%
“…Besides, methods for calculating LOD values have not been standardized. Therefore, comparison of the results published in the literature is hardly possible as most of the factors influencing the LOD differ from one paper to another (5,7,9,13).…”
Section: Discussionmentioning
confidence: 99%
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“…Mass spectrometric analysis, which provides molecular weight and characteristic fragmentation patterns, provides confirmation of antibacterials with retention and spectral characteristics. Several determination methods of CAP residues in urine, plasma, meat, egg, and milk by gas chromatography-mass spectrometry (GC-MS) (Gazzaniga et al, 1973;Janssen and Vanderhaeghe, 1973;Nakagawa et al, 1975;Keukens et al, 1992;Kijak, 1994;Borner et al, 1995) or liquid chromatography-mass spectrometry (Bories et al, 1983;Delepine and Sanders, 1992;Ramsey et al, 1989) have been reported so far. The detection limits of these determination methods were between 0.2 ppb and 0.5 ppm.…”
Section: Introductionmentioning
confidence: 99%
“…Injection sites contained even nine-fold higher levels at day 14 and 3.7 ± 3.7 ng/g at day 21, but no detectable levels at day 35. Delépine and Sanders (1992) treated three one-month-old calves with an i.v. dose of 25 mg/kg b.w.…”
Section: Ruminantsmentioning
confidence: 99%