1997
DOI: 10.1109/10.581938
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Determination of glucose concentrations in an aqueous matrix from NIR spectra using optimal time-domain filtering and partial least-squares regression

Abstract: We have investigated the use of a time-domain optimal filtering method to simultaneously minimize both the baseline variation and high-frequency noise in near-infrared (NIR) spectrophotometric absorption data of glucose dissolved in a simple aqueous (deionized water) matrix. By coupling a third-order (six-pole) digital Butterworth bandpass filter with partial least-squares (PLS) regression modeling, glucose concentrations were determined for a set of test data with a standard error of prediction (SEP) of 10.53… Show more

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Cited by 50 publications
(27 citation statements)
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“…The standard error of prediction (RMSEP) and the standard error of calibration (RMSEE) were adopted as error estimation parameters for both calibration and validation procedures22 …”
Section: Methodsmentioning
confidence: 99%
“…The standard error of prediction (RMSEP) and the standard error of calibration (RMSEE) were adopted as error estimation parameters for both calibration and validation procedures22 …”
Section: Methodsmentioning
confidence: 99%
“…To our knowledge, this is the first time LLER is combined with digital bandpass filtering for NIR spectroscopy. In this work, the digital Gaussian and Chebyshev bandpass filters have been used to suppress the high frequency components as well as the baseline variations which dominate the low frequency components in the raw spectra [18,19]. The digital bandpass filters are defined by two parameters [20,21], the centre frequency and the bandwidth.…”
Section: Ller Model Combined With Digital Bandpass Filteringmentioning
confidence: 99%
“…Because of serious overlapping of components spectrum within NIR range and collinearity problems between spectrum data, it is not desirable to setup calibration model and carry out prediction by using Univariate Linear Regression (ULR) and Multiple Linear Regression (MLR). Currently one of the popular multivariate analysis methods applied for glucose measurement is Partial Least Squares (PLS) [8][9][10] , which models both the X-and Y-matrices simultaneously to find the latent variables in X that will best predict the latent variables in Y. PLS method combines principle component analysis and regression analysis together, and it can overcome the collinearity problems between spectrum data. There is no limitation on the number of wavelength employed when setting up calibration model, all spectrum data can be used to set up calibration model.…”
Section: Beer's Lawmentioning
confidence: 99%