Abstract:A simple method for determining HF and U(\1) in a hydrolyzed solution of UF, hy alkalimetry is described. About l g of UF 6 was taken in a polytrifluoromonochloroethylene tube, and hydrolyzed with about 50 ml of water in a closed polyethylene bottle. Using a glass electrode, HF in the hydrolyzed solution was titrated potentiometrically with an alkali solution, after the U(\11) had been masked with ammonium sulfate. When the equivalence point for the free acid was reached, hydrogen peroxide was added to the sol… Show more
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