1936
DOI: 10.1021/ac50102a019
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Determination of Hydroxyl Groups in Organic Compounds

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Cited by 36 publications
(12 citation statements)
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“…However, a reaction similar to lOd may here play an important role. Free methyl and free acetoxy radicals attack the solvent as in equation 18 and to a very minor extent (if at all) the lead tetraacetate as in equations 15 and 16.…”
Section: Interpretation Of Resultsmentioning
confidence: 99%
See 1 more Smart Citation
“…However, a reaction similar to lOd may here play an important role. Free methyl and free acetoxy radicals attack the solvent as in equation 18 and to a very minor extent (if at all) the lead tetraacetate as in equations 15 and 16.…”
Section: Interpretation Of Resultsmentioning
confidence: 99%
“…124.5-125°). The isopropyl alcohol (0.0035 mole) was determined by the method of Freed and Wynne (18), and the carbanilic ester (m.p. 87-87.5°) was made.…”
Section: (Ch3c02mentioning
confidence: 99%
“…During the acetylation of glucose, acetic anhydride is almost always the reagent of choice, and the catalysts most frequently employed are zinc chloride [ 14 ] (or other Lewis acids), sodium acetate [ 15 ] and pyridine [ 16 ]. The acetylation of other sugars can be carried out under similar conditions.…”
Section: Introductionmentioning
confidence: 99%
“…Molecular weights were determined cryscopically in benzene. The weight in grams of substance containing one equivalent of hydroxyl (acetylation number) was determined by the method of Freed and Wynne (14).…”
Section: Introductionmentioning
confidence: 99%