1952
DOI: 10.1021/ac60067a035
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Determination of Insecticide Residues

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1953
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Cited by 5 publications
(3 citation statements)
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“…As previous work had shown (14) that Deniges reagent can be reduced by materials other than chrysanthemic acid without the formation of a colored precipitate, it was considered that the apparently specific color reaction of Denigfes reagent with chrysanthemic acid might give values uninfluenced to a substantial degree by extraneous material. It was also hoped to avoid errors likely to occur with pyrethrins in the AOAC 1947 Method and errors in spectrophotometric analysis in the ultraviolet range (3,15) caused by the presence of biologically inactive material, such as polymerized material and unsaturated fatty acid esters (8).…”
Section: Laboratorymentioning
confidence: 99%
“…As previous work had shown (14) that Deniges reagent can be reduced by materials other than chrysanthemic acid without the formation of a colored precipitate, it was considered that the apparently specific color reaction of Denigfes reagent with chrysanthemic acid might give values uninfluenced to a substantial degree by extraneous material. It was also hoped to avoid errors likely to occur with pyrethrins in the AOAC 1947 Method and errors in spectrophotometric analysis in the ultraviolet range (3,15) caused by the presence of biologically inactive material, such as polymerized material and unsaturated fatty acid esters (8).…”
Section: Laboratorymentioning
confidence: 99%
“…An infrared spectrophotometric method has been proposed for aldrin and dieldrin (68), a colorimetric procedure for piperonyl butoxide (92), an improved technique for dithiocarbamate residues permitting detection of less than 1 p.p.m. of the insecticide (114), and detection of pyrethrum in flour picked up in bags with pyrethrum-treated warp (169), and in p3rrethrum-coated paper bags (53).…”
Section: Insecticide Residuesmentioning
confidence: 99%
“…Edwards and Cueto (28) developed a procedure for the colorimetric estimation of pyrethrins on coated paper bags utilized for control in manufacture and for determining the stability of pyrethrins during storage. Schreiber and McClellan (116) developed a method to reduce the interference of fatty acids for the determination of insecticide residues found in flour from pyrethrin-treated bags. 1080, ANTU, AND WARFARIN Ramsey and Clifford (103,105) presented a method for the determination of monofluoroacetic acid in foods and biological materials.…”
Section: Rotenonementioning
confidence: 99%