Determination of water and hydrogen bonding in tris-[1-(2-methyl)aziridinyl] phosphine oxide by infrared and nuclear magnetic resonance spectrometry

Tompa, Albert S.; Barefoot, Rupert D.

doi:10.1021/ac60259a047

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1969

1974

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Cited by 3 publications

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“…Twenty per cent solutions were needed for HTPB-A and C prepolymers because their initial hydroxyl concentrations were only 0.5 to 0.7%. The hydroxyl content was determined using the 3615 cm-1 band by the peak height method with the base line drawn from 3700 to 3200 cm-1, and by graphical integration (8,9) of the area delimited by the absorption bands between 3700 to 3200 cm-1. The hydroxyl absorbance must be corrected for the interference of the antioxidant.…”

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confidence: 99%