Determination of zirconium in zirconium metal and zirconium powder by use of mandelic acid

Norwitz, George

doi:10.1016/s0003-2670(01)81713-x

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1967

2024

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Cited by 5 publications

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“…Gravimetric MethodsReagent: Material (References) Mandelic acid: Thermogravimetric study (1); Zr metal(375) …”

mentioning

confidence: 99%

Nonferrous metallurgy. II. Zirconium, hafnium, vanadium, niobium, tantalum, chromium, molybdenum, and tungsten

Bachman¹,

Banks²

1967

Anal. Chem.

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“…Gravimetric MethodsReagent: Material (References) Mandelic acid: Thermogravimetric study (1); Zr metal(375) …”

mentioning

confidence: 99%

Nonferrous metallurgy. II. Zirconium, hafnium, vanadium, niobium, tantalum, chromium, molybdenum, and tungsten

Bachman¹,

Banks²

1967

Anal. Chem.

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Development of analytical method for zirconium determination in U–Pu–Zr alloy samples

Mishra,

Rawat,

Thakur

et al. 2024

J Radioanal Nucl Chem

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The study focuses on developing a robust method for determining zirconium in U–Pu–Zr alloy samples, crucial for assessing fuel composition and ensuring uniformity. Using mandelic acid precipitation and spectrophotometric quantification with Arsenazo-III, the method achieves high sensitivity and reproducibility, crucial for handling microgram-levels of Pu. By optimizing conditions to maintain Pu in its + 3 oxidation state, interference during Zr precipitation is minimized. Comparative analyses with ICP-AES validate the accuracy and reliability of the results. This approach not only enhances analytical precision but also reduces radioactive waste, making it suitable for nuclear fuel characterization.

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Gravimetric Determinations

Mukherji

1970

Analytical Chemistry of Zirconium and Hafnium

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Determination of zirconium in zirconium metal and zirconium powder by use of mandelic acid

Cited by 5 publications

References 15 publications

Nonferrous metallurgy. II. Zirconium, hafnium, vanadium, niobium, tantalum, chromium, molybdenum, and tungsten

Nonferrous metallurgy. II. Zirconium, hafnium, vanadium, niobium, tantalum, chromium, molybdenum, and tungsten

Development of analytical method for zirconium determination in U–Pu–Zr alloy samples

Gravimetric Determinations

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