2017
DOI: 10.14233/ajchem.2017.20431
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Development and Validation of Piribedil in Tablet Dosage Form by HPLC: A QbD and OFAT Approach

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Cited by 4 publications
(5 citation statements)
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“…The LOD and LOQ were determined experimentally by calculating the concentrations yielding peaks to noise ratios of 3 : 1 (LOD) or 10 : 1 (LOQ) as stated by the USP [28]. The proposed and reference methods [29][30][31] were applied to determine the concentration of each drug either alone or in laboratory-prepared mixtures. By recognition of the high values of the percentage recoveries, and low values of t and F parameters [32], the accuracy of the proposed method could be easily proved (table 5).…”
Section: Methods Validationmentioning
confidence: 99%
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“…The LOD and LOQ were determined experimentally by calculating the concentrations yielding peaks to noise ratios of 3 : 1 (LOD) or 10 : 1 (LOQ) as stated by the USP [28]. The proposed and reference methods [29][30][31] were applied to determine the concentration of each drug either alone or in laboratory-prepared mixtures. By recognition of the high values of the percentage recoveries, and low values of t and F parameters [32], the accuracy of the proposed method could be easily proved (table 5).…”
Section: Methods Validationmentioning
confidence: 99%
“…Accuracy and precision data for the proposed HMLC method. studied drug parameter % found reference methods, % found[29][30][31] application of HMLC for the determination of the drugs in pure form Figures between parentheses are the tabulated t and F values at P = 0.05[32].…”
mentioning
confidence: 99%
“…Mohan et al reported an assay estimation method of piribedil in the finished dosage form [16] . Basis a careful review of the reported analytical method, we observed that the method's specificity was not ensured by injecting the major known degradation products to rule out any coelution with the parent compound (piribedil).…”
mentioning
confidence: 99%
“…Three different water-insoluble to water-soluble polymer ratios were optimized using a 3 2 full factorial design approach 18 . Coated LCDH granules were evaluated for powder properties such as bulk density, tapped density, Carr"s index, Hausner"s ratio and in-vitro disintegration time, invitro drug release studies, and in-vivo taste evaluation.…”
mentioning
confidence: 99%