Development of a strategy for a quick process for separation of volatile compounds in counter-current chromatography: purification of cinnamaldehyde from <i>Cinnamomum cassia</i> by high performance counter-current chromatography

Fan, Qing-Fei; Feng-mei, Huang; Zhou, Lanzhang; He, Wenxiang; Jiang, Xian; Na, Zhi; Gongpan, Pianchou; Hu, Huabin; Qin, Song

doi:10.1080/10826068.2021.1894444

Preparative Biochemistry & Biotechnology

2021

DOI: 10.1080/10826068.2021.1894444

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Development of a strategy for a quick process for separation of volatile compounds in counter-current chromatography: purification of cinnamaldehyde from Cinnamomum cassia by high performance counter-current chromatography

Qing-Fei Fan

Huang Feng-mei

Lanzhang Zhou

et al.

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2024

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Cited by 4 publications

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Recent trends in multidimensional countercurrent chromatography

Muhire,

Sun,

Zhang

et al. 2024

J of Separation Science

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Countercurrent chromatography (CCC) is a potent separation approach known for its remarkable efficiency and capacity in preparation. It's applied as a substitute or combined with different chromatographic techniques, resulting in its rebranding as multidimensional CCC (MDCCC). Numerous essential mixtures from natural products contain hundreds or thousands of distinct components of importance. These mix types are too complicated to separate in any reasonable time using a single CCC dimension. However, if a multidimensional technique is utilized, where a complex mixture is separated by an initial dimension, smaller fractions of that separation are gathered. Each fraction is studied individually; complex mixes can be resolved relatively quickly. Thus, several MDCCC separation features have been studied to demonstrate their advantages, limitations, and prospective capacity to separate exceedingly complex mixtures. In this review, MDCCC aspects, including principles, multiple columns system, multilayer coil J‐type, on‐line monitoring system, and applications, have been thoroughly_explored.

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Recent trends in multidimensional countercurrent chromatography

Muhire,

Sun,

Zhang

et al. 2024

J of Separation Science

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Prediction model for retention volumes of the three‐phase solvent system in high‐speed countercurrent chromatography

Muhire,

Zhang,

Sun

et al. 2024

J of Separation Science

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Owing to its ability to separate substances with a broad scope of polarities, exploring the three‐phase solvent systems (TPSSs) with high‐speed countercurrent chromatography is a topic of interest in separation science, and their retention volumes should be more concerned. This study primarily investigates the behavior of retention volumes while examining the isolation abilities of the TPSS in the technique above. We took standard compounds, including sophoricoside, Sudan red 7B, and rotenone, which have a broad range of polarity, for investigation in this study and separated them using different four‐liquid TPSSs made up of water, acetonitrile, methyl acetate, and n‐hexane (WAMH). Our findings show that the retention volumes gradually alter in response to changes in phase polarity within the proposed solvent systems. With TPSSs, we preliminarily studied compound isolation and the promising formula of their retention volumes. The proposed solvent systems WAMH in different ratios showed high correlations and adjusted correlation coefficients above 0.9978 and 0.9913 for the actual and calculated retention volumes. This study will be particularly beneficial for researchers focusing on countercurrent chromatography with TPSSs, as it offers valuable time‐saving insights.

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Towards the photocatalytic production of cinnamaldehyde with phosphorous-tailored graphitic-like carbon nitride

Quintana,

Picón,

Martín-Lara

et al. 2024

Applied Catalysis A: General

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Development of a strategy for a quick process for separation of volatile compounds in counter-current chromatography: purification of cinnamaldehyde from Cinnamomum cassia by high performance counter-current chromatography

Cited by 4 publications

References 20 publications

Recent trends in multidimensional countercurrent chromatography

Recent trends in multidimensional countercurrent chromatography

Prediction model for retention volumes of the three‐phase solvent system in high‐speed countercurrent chromatography

Towards the photocatalytic production of cinnamaldehyde with phosphorous-tailored graphitic-like carbon nitride

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