The results of a study on the effect of oxidation on the AP index and acidiry of three Nigerian coals are reported. The coals were oxidized in air over a period of 35 days at both 100 and 50°C. The heating value, slurry pH (acidity), and the AP index of three Nigerian coal sample were monitored as afunction of o.ridation rime. The results revealed a decrease in AP index and an increase in the acidity of all rhree coals with increase in oxidation time. The heating value of the coals was also reduced by the oxidation.