2007
DOI: 10.1117/12.725160
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Development of capillary Z-pinch discharge soft x-ray laser

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“…The yield of this reaction is not remarkable, yet is fairly good considering that this procedure is much less expensive and faster than that reported. [37] The only drawback of this reaction concerns the pH in its workup; indeed, pH values only slightly outside the range of 5-6 lead to drastic decreases in yield. The resolution of (AE)-2 was carried out by fractional crystallization from ethanol/water of the diastereomeric salts obtained with (S)-or (R)-1-(2-naphthyl)-ethylamine.…”
Section: Chemistrymentioning
confidence: 99%
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“…The yield of this reaction is not remarkable, yet is fairly good considering that this procedure is much less expensive and faster than that reported. [37] The only drawback of this reaction concerns the pH in its workup; indeed, pH values only slightly outside the range of 5-6 lead to drastic decreases in yield. The resolution of (AE)-2 was carried out by fractional crystallization from ethanol/water of the diastereomeric salts obtained with (S)-or (R)-1-(2-naphthyl)-ethylamine.…”
Section: Chemistrymentioning
confidence: 99%
“…The resolution of (AE)-2 was carried out by fractional crystallization from ethanol/water of the diastereomeric salts obtained with (S)-or (R)-1-(2-naphthyl)-ethylamine. [37] As an alternative to resolution, we tried to prepare (+)-2 and (À)-2 by the same procedure used for the racemate by starting from optically active 4-chloromandelic acid. Unfortunately, the reaction occurred with partial racemization; however, this synthetic method was useful for unambiguously assigning the absolute configuration to both isomers, given that the stereogenic center of optically active 4-chloromandelic acid was not involved in the reaction.…”
Section: Chemistrymentioning
confidence: 99%
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