Development of Cf/C-UHTC composite and study of its resistance to oxidation and ablation in high-speed high-enthalpy air plasma flow

Astapov, A.N.; Pogodin, V.A.; Sukmanov, I.V.; Zhestkov, B.E.; Prokofiev, M.V.

doi:10.1016/j.ijlmm.2024.02.003

International Journal of Lightweight Materials and Manufacture

2024

DOI: 10.1016/j.ijlmm.2024.02.003

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Development of Cf/C-UHTC composite and study of its resistance to oxidation and ablation in high-speed high-enthalpy air plasma flow

A.N. Astapov,

V.A. Pogodin,

I.V. Sukmanov

et al.

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Utilization of handheld LIBS and XRF analyzers for impurity detection in 3D-printed ultra-high-temperature ceramics

Emrick,

Cochrane,

Rao

2024

Appl. Opt.

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In this study, we implement handheld laser-induced breakdown spectroscopy (LIBS) and X-ray fluorescence (XRF) analyzers to detect elemental impurities in additively manufactured ultra-high-temperature ceramics (UHTCs). Spectral data were collected from digital light processing (DLP) 3D-printed alumina (Al2O3) samples at various processing stages. These stages included high-temperature debinding and sintering phases used to bake out organic impurities and improve grain cohesion of the ceramic. Spectral analysis revealed the presence of organic impurities such as H and C together, with inorganic impurities such as Na, Si, Ca, and Fe. A reduction in elemental impurities in the spectra was observed as the ceramic samples were processed, validating the effectiveness of handheld analyzers for in situ rapid impurity detection and quality control in the manufacturing of 3D-printed UHTCs.

show abstract

Utilization of handheld LIBS and XRF analyzers for impurity detection in 3D-printed ultra-high-temperature ceramics

Emrick,

Cochrane,

Rao

2024

Appl. Opt.

View full text Add to dashboard Cite

show abstract

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Development of Cf/C-UHTC composite and study of its resistance to oxidation and ablation in high-speed high-enthalpy air plasma flow

Cited by 1 publication

References 26 publications

Utilization of handheld LIBS and XRF analyzers for impurity detection in 3D-printed ultra-high-temperature ceramics

Utilization of handheld LIBS and XRF analyzers for impurity detection in 3D-printed ultra-high-temperature ceramics

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