“…23 Finally, a sample of pure cellulose, giving the same NMR and X-ray photoelectron spectroscopy signals as LS, 24 was studied as a reference. It exhibited three diffraction lines, in agreement with Abou-Sekkina et al 25 (JCPDS 50-2241) and Deraman et al 26 in terms of position and relative intensities: a broad asymmetric peak at 2y ¼ 15 , corresponding to amorphous cellulose, a sharp peak at 2y ¼ 22.6 , and a small peak at 34 , corresponding to crystalline cellulose.…”