Development of magnetic graphene @hydrophilic polydopamine for the enrichment and analysis of phthalates in environmental water samples

Wang, Ding; Song, Guoxin; Deng, Chunhui

doi:10.1016/j.talanta.2014.10.014

Cited by 50 publications

(23 citation statements)

References 38 publications

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“…The new method developed in this study was compared with some previously reported methods for the extraction and determination of PAEs (Table 3). The proposed method demonstrated comparable LODs, LOQs, and recoveries compared to other reported MSPE methods in water samples (Wang et al., 2015; Ye et al., 2014; Zare Jeddi, Ahmadkhaniha, Yunesian, & Rastkari, 2014). Moreover, the method developed in the present study exhibited lower LODs than other extraction methods that use dispersive‐SPE with colloidal graphene (Wu et al., 2013), and SBSE with polydimethylsiloxane (Si et al., 2016).…”

Section: Resultsmentioning

confidence: 61%

“…Graphene oxide has attracted interest as a promising sorbent material due to its hydrophilicity, ultrahigh surface area, and high dispersion stability (González‐Sálamo, Socas‐Rodríguez, Hernandez‐Borges, & Rodríguez‐Delgado, 2016). In this regard, several PAEs also have been determined using graphene oxide (Wang, Song, & Deng, 2015; Wu et al., 2013; Ye, Liu, & Chen, 2014); however, nanoscale materials possess some disadvantages in terms of their large‐scale synthesis and hazards associated with their postadsorption disposal (Shaida, Dutta, & Sen, 2018). Consequently, the use of inexpensive and naturally derived materials is more appropriate for the adsorption of environmental pollutants.…”

Section: Introductionmentioning

confidence: 99%

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Magnetic solid‐phase extraction based on magnetic carbon particles from coffee grounds for determining phthalic acid esters in plastic bottled water

Song

Lim

Choi

et al. 2020

Journal of Food Science

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Newly developed magnetic carbon particles prepared from coffee grounds were used as the sorbent for the magnetic solid-phase extraction of eight phthalic acid esters (PAEs) from plastic bottled water prior to their analysis by GC-MS. The method, which uses coffee-ground particles coated with iron oxide, was validated, and exhibited linearities for the eight PAEs, with coefficients of determination above 0.998 in the 0.005 to 0.1 mg/L concentration range. Limits of detection and limits of quantification of 0.00003 to 0.002 mg/L and 0.0001 to 0.005 mg/L, respectively, were achieved, with recoveries (%) ranging between 77% and 120%, and relative standard deviations for intra-and interday precisions below 16.3% at three fortification levels. No PAE residues were detected when the developed and validated method was applied to 10 real plastic bottled water samples. Taken together, the developed magnetic solid-phase extraction method is a useful tool for monitoring phthalate esters in aqueous samples.Practical Application: The development of a new, inexpensive, and efficient magnetic sorption material derived from spent coffee grounds, and its ability to determine phthalate esters in aqueous solutions was described by GC-MS/MS. The developed magnetic solid-phase extraction method is a useful tool for monitoring phthalate esters in aqueous samples.

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Section: Resultsmentioning

confidence: 61%

Section: Introductionmentioning

confidence: 99%

Magnetic solid‐phase extraction based on magnetic carbon particles from coffee grounds for determining phthalic acid esters in plastic bottled water

Song

Lim

Choi

et al. 2020

Journal of Food Science

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“…Importantly, it is suitable for handling large volumes of samples . Recently, MSPE with HPLC and GC has been successfully applied to the separation, concentration, and analysis of various organic pollutants and inorganic metal ion contaminants in environmental water .…”

Section: Introductionmentioning

confidence: 99%

Analysis of microcystins using high‐performance liquid chromatography and magnetic solid‐phase extraction with silica‐coated magnetite with cetylpyridinium chloride

Lian

Wang

et al. 2017

J of Separation Science

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Microcystins (MCs), produced by freshwater cyanobacteria, can be serious water pollutants, so it is important to monitor their concentration in drinking water. We have developed a method for rapid and accurate determination of microcystin levels in environmental water, using magnetic solid-phase extraction and high-performance liquid chromatography with UV detection. The magnetic composite material, which was combined with cetylpyridinium chloride, was prepared by hydrothermal synthesis. The optimal extraction of microcystins in water sample was achieved by optimizing the amount of adsorbent, time of adsorption, ratio of eluting solvent, and volume of eluent. Under the optimal conditions, the limit of detection of MC-LR was 0.001 μg/L, and the limit of quantification was 0.0028 μg/L. The limit of detection of MC-RR was 0.001 μg/L, and the limit of quantification was 0.003 μg/L. These values are far lower than those established by the International Health Organization for the maximum concentration of microcystins in drinking water. The magnetic solid-phase extraction adsorbent used in this method has the advantages of simple preparation, low price, and easy solid-liquid separation, and it can be used for the rapid and sensitive monitoring of trace microcystins in environmental water samples.

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“…But these procedures are always laborious, time-consuming and sometimes requiring large amounts of organic solvents [14]. In order to avoid these drawbacks, solid-phase microextraction, stir bar sorptive extraction and magnetic solid-phase extraction are used in the analysis of BPs [15][16][17].…”

Section: Introductionmentioning

confidence: 99%

Preparation of magnetic graphene @polydopamine @Zr-MOF material for the extraction and analysis of bisphenols in water samples

Wang

Deng

2015

Talanta

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Development of magnetic graphene @hydrophilic polydopamine for the enrichment and analysis of phthalates in environmental water samples

Cited by 50 publications

References 38 publications

Magnetic solid‐phase extraction based on magnetic carbon particles from coffee grounds for determining phthalic acid esters in plastic bottled water

Magnetic solid‐phase extraction based on magnetic carbon particles from coffee grounds for determining phthalic acid esters in plastic bottled water

Analysis of microcystins using high‐performance liquid chromatography and magnetic solid‐phase extraction with silica‐coated magnetite with cetylpyridinium chloride

Preparation of magnetic graphene @polydopamine @Zr-MOF material for the extraction and analysis of bisphenols in water samples

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