“…It is known that metal acetates as well as metal alkoxides are easily dissolved in mixed solvents such as ethanol, ethylene glycol and 2-methoxy ethanol [5]. Several preparation methods have been reported in literature to synthesize nanocrystalline pyrochloretype powders, such as: solid-state reaction [6], propionic acid routes [7], malate [8] coprecipitation [9], sol-gel [10], modified Pechini [11] and citrate [12].…”