Ni 0.4 Mg 0.6 Fe 2 O 4 Ceramic samples were prepared by conventional double sintering approach and sintered at 1300 o C/4 h. These ferrites are further characterized using X-ray diffractometer. The diffraction study reveals that the present compound shows perfect single phase cubic spinel structure. In addition, the behavior of distinct electrical properties such as dielectric constant (ε'), dielectric loss (ε") and ac-conductivity (ζ ac ) as a function frequency as well as temperature is analyzed using the LCR controller.