Dimethylformamid [MAK Value Documentation in German language, 1992]

doi:10.1002/3527600418.mb6812d0018

The MAK‐Collection for Occupational Health and Safety 2012

DOI: 10.1002/3527600418.mb6812d0018

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Dimethylformamid [MAK Value Documentation in German language, 1992]

Abstract: Veröffentlicht in der Reihe Gesundheitsschädliche Arbeitsstoffe , 18. Lieferung, Ausgabe 1992 Der Artikel enthält folgende Kapitel: Allgemeiner Wirkungscharakter Angaben zur Pharmakokinetik Erfahrungen beim Menschen Zusammenfassung Tierexperimentelle Befunde Akute und subakute Toxizi… Show more

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3‐Methyl‐5‐isopropylhydantoin als Hämoglobinaddukt desN,N‐Dimethylformamids und Methylisocyanats [Biomonitoring Methods in German Language, 2015]

Käfferlein

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Leng³

et al. 2016

The MAK‐Collection for Occupational Health and Safety

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The analytical method describes the specific determination of 3‐methyl‐5‐isopropylhydantoin (MIH), a hemoglobin adduct of N,N‐dimethylformamide. Following addition of 13 C 5 , 15 N‐3‐methyl‐5‐isopropylhydantoin ( 13 C 5 , 15 N‐MIH) as internal standard, isolated globin is subjected to acid hydrolysis for one hour at 110deg;C. After pH adjustment (pH 3–5) the hydrolysate is extracted twice with ethyl acetate. The combined extracts are washed with sodium hydrogen carbonate solution and dried under a stream of nitrogen. The residue is dissolved in ethyl acetate. An aliquot of the solution is analyzed using GC–MS. For calibration purposes, calibration standards are prepared in pooled globin. They are processed in the same way as the samples to be analyzed.

show abstract

3‐Methyl‐5‐isopropylhydantoin als Hämoglobinaddukt desN,N‐Dimethylformamids und Methylisocyanats [Biomonitoring Methods in German Language, 2015]

Käfferlein

Angerer

Leng³

et al. 2016

The MAK‐Collection for Occupational Health and Safety

View full text Add to dashboard Cite

show abstract

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Dimethylformamid [MAK Value Documentation in German language, 1992]

Cited by 1 publication

References 71 publications

3‐Methyl‐5‐isopropylhydantoin als Hämoglobinaddukt desN,N‐Dimethylformamids und Methylisocyanats [Biomonitoring Methods in German Language, 2015]

3‐Methyl‐5‐isopropylhydantoin als Hämoglobinaddukt desN,N‐Dimethylformamids und Methylisocyanats [Biomonitoring Methods in German Language, 2015]

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