Distillation

Rose, Arthur

doi:10.1021/ac60037a015

Anal. Chem.

1950

DOI: 10.1021/ac60037a015

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Distillation

Arthur Rose¹

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1950

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Volumetric Determination of Small Amounts of Iridium

Cluett¹

1950

Can. J. Res.

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A volumetric procedure is described for determining small amo-unts of iridium (from 2 to 20 mgm.). A solution of the metal is heate-d to dense fumes with sulphuric acid, codled, dilr,t"d rvith water, and then oxidized lvith an excess of cerium (IV)'sulphate solution. The resultant solution is titrated rvith a standard 0.01 N iron (Ii) sulphate solution, the course of the titration being followed potentiometrically. in solutions containing other platinum metals it has been iound possible to determine iridium directlf in some cases by this.procedure; in other cases it w'as found necessary to remove osmium as the volatile tetroxide prior to oxidizing with cerium (I\i) sulphate. The method.is probably less accurale than exisLinlg gravimetric prtcedrires. but offer' considerable advanrage in simplicity.

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Volumetric Determination of Small Amounts of Iridium

Cluett¹

1950

Can. J. Res.

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Distillation

Cited by 1 publication

References 18 publications

Volumetric Determination of Small Amounts of Iridium

Volumetric Determination of Small Amounts of Iridium

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