“…This porous structure is highly desirable for enhanced electrochemical reaction kinetics in supercapacitors due to the large surface area, easy access to the electrolyte, and reduced mass and charge diffusion distances [11]. Although the electrodeposition of Co(OH) 2 has been extensively studied under different conditions through a variation of synthesis parameters such as applied current density and potential as well as bath concentration, pH, and temperature [12][13][14], the use of pulse current (PC) for the deposition of Co(OH) 2 has not been reported in the literature. The additional operating parameters of PC such as current-on time (T on ), current-off time (T off ), duty cycle (h), and frequency (f) offer a facile, direct, and effective way to further precisely control the morphology of the electrodeposited film.…”