Dyeing of cotton fabric with a reactive disperse dye in supercritical carbon dioxide

Long, Jia‐Jie; Xiao, Guodong; Xu, Hongmei; Wang, Ling; Cui, Chuang-Long; Liu, Jing; Yang, Maohua; Wang, Ke; Chen, Chen; Ren, Yi-Meng; Luan, Tao; Ding, Zhi‐Fang

doi:10.1016/j.supflu.2012.05.002

Cited by 76 publications

(33 citation statements)

References 16 publications

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“…Furthermore, as shown in Figure 3, the carbon atoms C- (1)(2)(3)(4)(5)(6)(7)(8)(9)(10)(11)(12)(13)(14) from the anthraquinone ring were detected with chemical shifts (δ) ranging from 185.20 ppm to 113.60 ppm. The carbon atoms C- (15)(16) from the methyl group of the bridge were also detected with chemical shifts (δ) at 39.73 ppm and 49.77 ppm, respectively.…”

Section: Nmr Spectral Analysismentioning

confidence: 98%

“…The coloration of cotton and wool fabrics was performed with the synthesized SCF-X-ANR02 dye in supercritical carbon dioxide fluid at a system pressure of 25.0 MPa and a temperature of 110.0 o C for 60.0 min, by utilizing a self-built supercritically dyeing system in our research group as described elsewhere [7,13,28]. A 2.0 g of cotton or wool fabric sample with a dosage of the SCF-X-ANR02 dye powder at 1.5% o.m.f.…”

Section: Coloration Of Cotton and Wool With The Scf-x-anr02 Dye In Scmentioning

confidence: 99%

“…(on the mass of fabric) and a supercritical bath ratio at 1:150 were used during the coloration process. The other procedures as well as operations were referenced to the literature reports [7,13,28].…”

Section: Coloration Of Cotton and Wool With The Scf-x-anr02 Dye In Scmentioning

confidence: 99%

“…Co., Ltd., Reston, USA) was used to evaluate the color characteristics and the color intensity of K/S values for the dyed cotton and wool fabrics, with a simulated D 65 light source lamp and a 10˚ visual angle. Moreover, the Kubelka-Munk equation was also applied to achieve the K/S and values at a maximum absorption wavenumber (λ max ) of 505.0 nm and 500.0 nm for the dyed cotton and wool samples, respectively, according to the literature [7,13,28]. A leveling property of the synthesized SCF-X-ANR02 dye on the cotton and wool fabric substrates were also assessed by utilizing a standard deviation (σ K/S ) of the K/S values according to our previous work [28].…”

Section: Color and Fastness Evaluations For The Dyed Substratesmentioning

confidence: 99%

“…As well known, supercritical dyeing of textiles is a green and sustainable technology by utilizing supercritical carbon dioxide as media, and now can be commercially applied in polyester and other synthesized fiber substrates in recent years [1][2][3][4][5]. However, supercritical carbon dioxide fluid is a typical non-polar medium, so the hydrophilic and/or ionic dyestuffs are not applicable in this kind of medium [6][7][8][9][10]. Consequently, there is really a little difficult to apply this green and cleaner coloration technology to hydrophilic fibers, such as natural fibers, by employing their conventional dyestuffs as like in water bath.…”

Section: Introductionmentioning

confidence: 99%

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Synthesis of a Special Dye SCF-X-ANR02 and its Dyeing Property in Green Media of Supercritical Carbon Dioxide

Sun¹

2018

Int. J. Green Technol.

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A special dye of SCF-X-ANR02 involving an anthraquinonoid chromophoric system and a new bridge group linked with a dichlorotriazine reactive group was designed and developed at the first time, in order to apply for dyeing cotton and wool substrates with a green technology in supercritical carbon dioxide. Moreover, the dyeing property of the obtained dye was also investigated and compared on cotton and wool fabrics. The results show that the designed SCF-X-ANR02 dye was successfully synthesized by employing an Ullmann reaction with copper as catalyst, as well as a subsequent condensation reaction for bonding a reactive group. Moreover, the chemical structure of the SCF-X-ANR02 dye was well characterized and confirmed by Fourier transform infrared FTIR analysis, nuclear magnetic resonance spectroscopy of 1 H NMR and 13 C NMR, and liquid chromatography-mass spectrometry (LC-MS). The coloration results show that good dyeing properties, such as uptake and leveling behaviors, as well as color fastness were observed on cotton and wool fabrics in supercritical carbon dioxide dyeing media.

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